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Chemical Structure| 150374-98-4 Chemical Structure| 150374-98-4

Structure of 150374-98-4

Chemical Structure| 150374-98-4

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Product Details of [ 150374-98-4 ]

CAS No. :150374-98-4
Formula : C27H28N2O7S
M.W : 524.59
SMILES Code : CC(C)(C)C(OC1=CC=C(S(=O)(NC2=CC=CC=C2C(NCC(OCC3=CC=CC=C3)=O)=O)=O)C=C1)=O
MDL No. :MFCD11655948

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Application In Synthesis of [ 150374-98-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 150374-98-4 ]

[ 150374-98-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 150374-99-5 ]
  • benzyl 2-(2-aminobenzamido)acetate [ No CAS ]
  • [ 150374-98-4 ]
YieldReaction ConditionsOperation in experiment
89.5% With pyridine; In dichloromethane; at 20 - 25℃; for 3.5h; Benzyl 2- (2-aminobenzamido) acetate (10) (1.4 g, 0.0049 mol) prepared according to Example 8 was dissolved in dichloromethane (9 ml) and pyridine(1.2 g, 0.015 mol)Of the suspension,4- (chlorosulfonyl) phenyl (6) pivalate prepared according to Example 4(1.4 g, 0.0049 mol) in dichloromethane (7 ml)At 20 to 25 C. in about 30 minutes. The mixtureWhile monitoring by HPLC,Stirring is continued for 3 hours. After completion of the reaction,Water (10 ml) was added,Separate the phases. The organic phase was washed with waternext,Wash with 10% hydrochloric acid (10 ml) and saturated aqueous NaCl solution (10 ml). The mixture was crystallized from isopropyl ether (10 ml)Filtered,Dry at 40 C under reduced pressure. 2.3 g (89.5%) of a white solid are obtained.
 

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