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Chemical Structure| 1467061-56-8 Chemical Structure| 1467061-56-8

Structure of 1467061-56-8

Chemical Structure| 1467061-56-8

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Product Details of [ 1467061-56-8 ]

CAS No. :1467061-56-8
Formula : C17H19BO3
M.W : 282.14
SMILES Code : OC1=CC=CC=C1C2=CC=C(B3OCC(C)(C)CO3)C=C2
MDL No. :MFCD28133800

Safety of [ 1467061-56-8 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319
Precautionary Statements:P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330

Application In Synthesis of [ 1467061-56-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1467061-56-8 ]

[ 1467061-56-8 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1219741-54-4 ]
  • [ 126-30-7 ]
  • [ 1467061-56-8 ]
YieldReaction ConditionsOperation in experiment
99% In 1,4-dioxane; at 210.0℃; for 1.0h;Microwave irradiation; A mixture of 2,2-dimethylpropane-1,3-diol (4.0 g, 38 mmol) and 4'-(4,4,5,5-tetramethyl-[1,3,2]dioxaborolan-2-yl)biphenyl-2-ol (1.0 g, 3.4 mmol) in 1,4-dioxane (2 mL) was subjected to microwave irradiation at 210 C. for 1 hour. The cooled reaction mixture was partitioned between water (50 mL) and 1:1 EtOAc/heptane (25 mL:25 mL). The organic layer was washed with water (30 mL) and brine (30 mL), dried over Na2SO4 and concentrated in vacuo to give the title compound (0.95 g, 99% yield). GC/MS, M=282 at 5.31 min. 1H NMR (500 MHz, CDCl3) delta 7.94 (d, J=7.81 Hz, 2H), 7.48 (d, J=7.81 Hz, 2H), 7.31-7.26 (m, 2H), 7.03-6.98 (m, 2H), 3.82 (s, 4H), 1.08-1.04 (m, 6H).
 

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