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Chemical Structure| 1437306-55-2 Chemical Structure| 1437306-55-2

Structure of 1437306-55-2

Chemical Structure| 1437306-55-2

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Product Details of [ 1437306-55-2 ]

CAS No. :1437306-55-2
Formula : C34H22N2
M.W : 458.55
SMILES Code : C1(NC2=C3C=C(C4=CC5=C(C=C4)N(C6=CC=CC=C6)C7=C5C=CC=C7)C=C2)=C3C8=CC=CC=C8C=C1
MDL No. :N/A

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Application In Synthesis of [ 1437306-55-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1437306-55-2 ]

[ 1437306-55-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 854952-58-2 ]
  • [ 1698-16-4 ]
  • [ 1437306-55-2 ]
YieldReaction ConditionsOperation in experiment
88.7% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In ethanol; water; toluene; for 12h;Reflux; After introducing compound A (10-bromo-7H-benzo[cjcarbazole) (16 g, 54 mmol), (9-phenyl-9H-carbazol-3-yl)boronic acid (17 g, 59.4 mmol), Pd(PPh3)4 (3.1 g, 2.7 mmol), K2C03 (25.7 g, 108 mmol), distilled water (50 mL), toluene (250 mL), and ethanol(EtOH)(50 mL) in a flask, the mixture was stirred under reflux for 12 hours. After cooling to room temperature, the mixture was extracted with EA and distilled water, dried with magnesium sulfate, distilled under reduced pressure, and purified by column chromatography to obtain compound B(1 0-(9-phenyl-9H-carbazol-3-yl)-7H-benzo[cj carbazole) (22 g, yield: 88.7%).
 

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