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Chemical Structure| 1427002-41-2 Chemical Structure| 1427002-41-2

Structure of 1427002-41-2

Chemical Structure| 1427002-41-2

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Product Details of [ 1427002-41-2 ]

CAS No. :1427002-41-2
Formula : C48H30N6
M.W : 690.79
SMILES Code : C1(C2=CC=CN=C2)=C(C3=CC=CN=C3)C=C4C5=CC(C6=CC=CN=C6)=C(C7=CC=CN=C7)C=C5C8=CC(C9=CC=CN=C9)=C(C%10=CC=CN=C%10)C=C8C4=C1

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Application In Synthesis of [ 1427002-41-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1427002-41-2 ]

[ 1427002-41-2 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 82632-80-2 ]
  • [ 329214-79-1 ]
  • [ 1427002-41-2 ]
  • 2
  • [ 82632-80-2 ]
  • [ 1692-25-7 ]
  • [ 1427002-41-2 ]
YieldReaction ConditionsOperation in experiment
26% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate; In ethanol; toluene; for 28h;Inert atmosphere; Reflux; Obtained 2,3,6,7,10,11-hexa-bromo triphenylene 3.46g, and 3-pyridine boronic acid 4.0g, 2Maqueous solution of potassium carbonate 22.4ml, tetrakis (triphenylphosphine) palladium (0)0.57 g, toluene 180 ml, of ethanol 45ml and heated in addition to the reaction vessel wasreplaced with nitrogen, it was refluxed with stirring for 28 hours. After cooling to roomtemperature and added water 100 ml, chloroform 500 ml, was collected and the organic layer byperforming a liquid separation operation. The organic layer was washed with water 100 ml, driedover anhydrous magnesium sulfate to give the crude product by concentration. The resultingcrude product was purified by performing recrystallization from 1,2-dichlorobenzene,2,3,6,7,10,11 class of hexa (pyridin-3-yl) triphenylene (Compound 2) White obtained powder0.9g (26% yield).
 

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