Home Cart Sign in  
Chemical Structure| 1415638-13-9 Chemical Structure| 1415638-13-9

Structure of 1415638-13-9

Chemical Structure| 1415638-13-9

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1415638-13-9 ]

CAS No. :1415638-13-9
Formula : C5H7BrN2O
M.W : 191.03
SMILES Code : OCC1=C(N(N=C1)C)Br
MDL No. :MFCD28140435
InChI Key :DYXXSYMFUPNKBH-UHFFFAOYSA-N
Pubchem ID :84662962

Safety of [ 1415638-13-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H335
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338

Application In Synthesis of [ 1415638-13-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1415638-13-9 ]

[ 1415638-13-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 105486-72-4 ]
  • [ 1415638-13-9 ]
YieldReaction ConditionsOperation in experiment
99% Example 64-(Azetidin-1 -y I ) -3 -{ 5 -[4 -(d if luoromethyl)phenyl]-1 -methyl-1 H-pyrazol-4-yl}-1 -methyl-1 H- pyrazolo[3,4-d]pyrimidine6 C29 Step 1: Synthesis of (5-bromo-1-methyl-1H-pyrazol-4-yl)methanol (C23)A solution of ethyl 5-bromo-1 -methyl-1 /- -pyrazole-4-carboxylate (2.00 g, 8.58 mmol) in tetrahydrofuran (30 mL) at 0 C was treated with diisobutylaluminum hydride (1 M solution in tetrahydrofuran, 18.9 mL, 18.9 mmol), and the mixture was allowed to warm to roomtemperature and stir for 18 hours. Saturated aqueous sodium potassium tartrate solution was added, and stirring was continued for 4 hours. The aqueous layer was extracted with ethyl acetate, and the combined organic layers were dried over magnesium sulfate, filtered, and concentrated under reduced pressure. Purification via silica gel chromatography (Eluent: 100:1 ethyl acetate / methanol) afforded the product. Yield: 1 .63 g, 8.53 mmol, 99%. LCMS m/z 192.9 (M+1 ). H NMR (400 MHz, CDCI3) delta 2.44 (s, 1 H), 3.84 (s, 3H), 4.48 (s, 2H), 7.51 (s, 1 H).
 

Historical Records

Categories

Related Parent Nucleus of
[ 1415638-13-9 ]

Pyrazoles

Chemical Structure| 1393583-34-0

A441493 [1393583-34-0]

5-Bromo-1,4-dimethyl-1H-pyrazole

Similarity: 0.89

Chemical Structure| 54367-67-8

A490422 [54367-67-8]

5-Bromo-1-methyl-1H-pyrazole-4-carboxylic acid

Similarity: 0.87

Chemical Structure| 1269293-80-2

A932093 [1269293-80-2]

5-Bromo-1-methyl-1H-pyrazole-4-carbonitrile

Similarity: 0.84

Chemical Structure| 1374257-82-5

A378298 [1374257-82-5]

(5-Bromo-1-(tert-butyl)-1H-pyrazol-4-yl)methanol

Similarity: 0.83

Chemical Structure| 1374257-91-6

A272564 [1374257-91-6]

(5-Bromo-1-isopropyl-1H-pyrazol-4-yl)methanol

Similarity: 0.83