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Chemical Structure| 1403329-96-3 Chemical Structure| 1403329-96-3

Structure of 1403329-96-3

Chemical Structure| 1403329-96-3

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Product Details of [ 1403329-96-3 ]

CAS No. :1403329-96-3
Formula : C8H7BrF2OS
M.W : 269.11
SMILES Code : CSC1=CC=C(Br)C(OC(F)F)=C1
MDL No. :MFCD28738115

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Application In Synthesis of [ 1403329-96-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1403329-96-3 ]

[ 1403329-96-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 954235-83-7 ]
  • [ 5188-07-8 ]
  • [ 1403329-96-3 ]
YieldReaction ConditionsOperation in experiment
In N,N-dimethyl-formamide; at 60.0℃; for 1.0h; Intermediate Example Int 17.21 -bromo-2-(dif luoromethoxy)-4-(methy Isu Ifany l)benzene To a stirred solution of Int 17.1 (1 .0 g) in DMF (9.5 mL) was added sodium methanethiolate (460 mg). The mixture was stirred for 1 h at 60 C. The mixture was cooled to r.t., water (150 mL) was added and the mixture was extracted twice with ethyl acetate. The organic layer was washed with saturated sodium chloride solution, dried (sodium sulfate) and the solvent was removed in vacuum. Silica gel chromatography gave 850 mg of the title compound.
 

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