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Chemical Structure| 1368310-81-9 Chemical Structure| 1368310-81-9

Structure of 1368310-81-9

Chemical Structure| 1368310-81-9

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Product Details of [ 1368310-81-9 ]

CAS No. :1368310-81-9
Formula : C9H9N3O2
M.W : 191.19
SMILES Code : O=C(C1=CC=C2NC(NC)=NC2=C1)O
MDL No. :MFCD24502732
InChI Key :STZFNUKQFCVIQM-UHFFFAOYSA-N
Pubchem ID :59066917

Safety of [ 1368310-81-9 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H315-H319-H335
Precautionary Statements:P261-P305+P351+P338

Application In Synthesis of [ 1368310-81-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1368310-81-9 ]

[ 1368310-81-9 ] Synthesis Path-Downstream   1~4

  • 1
  • [ 1374258-49-7 ]
  • [ 1368310-81-9 ]
YieldReaction ConditionsOperation in experiment
90% With hydrogenchloride; In water;Reflux; 3 N Aqueous hydrochloric acid (14 mL, 42 mmol) was added to methyl 2-(methylamino)-1H-benzo[d]imidazole-5-carboxylate (2.9 g, 14 mmol) and the reaction was stirred at reflux overnight. The reaction was concentrated to give the title compound (2.4 g, 90%) as a yellow solid. 1H NMR (400 MHz, CD3OD, delta): 7.96-8.00 (m, 2H), 7.40 (d, J=8.4 Hz, 1H), 3.10 (s, 3H).
90% With hydrogenchloride; In water;Reflux; Step 2. 2-(methylamino)-1H-benzo[d]imidazole-5-carboxylic acid 3 N Aqueous hydrochloric acid (14 mL, 42 mmol) was added to methyl 2-(methylamino)-1H-benzo[d]imidazole-5-carboxylate (2.9 g, 14 mmol) and the reaction was stirred at reflux overnight. The reaction was concentrated to give the title compound (2.4 g, 90%) as a yellow solid. 1H NMR (400 MHz, CD3OD, delta): 7.96-8.00 (m, 2H), 7.40 (d, J=8.4 Hz, 1H), 3.10 (s, 3H).
  • 2
  • [ 36692-49-6 ]
  • [ 1368310-81-9 ]
  • 3
  • [ 1374258-50-0 ]
  • [ 1368310-81-9 ]
  • 4
  • [ 619-05-6 ]
  • [ 1368310-81-9 ]
 

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Technical Information

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