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Chemical Structure| 13424-80-1 Chemical Structure| 13424-80-1

Structure of 13424-80-1

Chemical Structure| 13424-80-1

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Product Details of [ 13424-80-1 ]

CAS No. :13424-80-1
Formula : C9H18N2O2
M.W : 186.25
SMILES Code : O=C(N(C)C)CCCC(N(C)C)=O

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Application In Synthesis of [ 13424-80-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 13424-80-1 ]

[ 13424-80-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 2873-74-7 ]
  • [ 543-20-4 ]
  • [ 111-50-2 ]
  • [ 124-40-3 ]
  • [ 13424-80-1 ]
  • [ 3644-93-7 ]
  • [ 7334-51-2 ]
YieldReaction ConditionsOperation in experiment
71.87%Chromat.; 13.31%Chromat.; 13.49%Chromat. With triethylamine; In toluene; at -10 - 20℃; for 2h; Procedure B: Formation of Diamide (as a Mixture) by Reaction with a Dialkylamine Toluene and triethylamine are loaded and cooled to -10 C. The dialkylamine is then loaded in liquid form. The acid dichloride (as a mixture), diluted in toluene is then added slowly while maintaining the temperature below +10 C. The mixture is then stirred for two hours at room temperature. The salts formed during the reaction are then filtered off and washed with ethyl acetate. The thereby obtained filtrate is then evaporated on the rotary evaporator in order to obtain the reaction raw product. The final product is finally obtained after distillation under reduced pressure. Raw product=729 g (brown liquid) Final product=574 g (slightly yellow liquid) GC analysis (surface area)>98% (sum of the isomers) The obtained product is analyzed by gas chromatography. The analysis indicates (as a peak surface area): It is also noticed that it is free of crystals at these temperatures.
 

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