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Chemical Structure| 1321613-04-0 Chemical Structure| 1321613-04-0

Structure of 1321613-04-0

Chemical Structure| 1321613-04-0

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Product Details of [ 1321613-04-0 ]

CAS No. :1321613-04-0
Formula : C14H17BCl2O4
M.W : 331.00
SMILES Code : O=C(OC)C1=C(Cl)C=C(B2OC(C)(C)C(C)(C)O2)C=C1Cl
MDL No. :MFCD20441900
InChI Key :JQJYCPNGBPJIFX-UHFFFAOYSA-N
Pubchem ID :56776843

Safety of [ 1321613-04-0 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H312-H332
Precautionary Statements:P261-P264-P270-P271-P280-P301+P312-P302+P352-P304+P340-P330-P363-P501

Application In Synthesis of [ 1321613-04-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1321613-04-0 ]

[ 1321613-04-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 73183-34-3 ]
  • [ 232275-53-5 ]
  • [ 1321613-04-0 ]
YieldReaction ConditionsOperation in experiment
57% With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In 1,4-dioxane; at 80℃; To a solution of 0188-1 (500 mg, 1.76 mmol) in dioxane (10 mL) was added bis(pinacolato)diboron (894 mg, 3.52 mmol), K2CO3 (486 mg, 3.52 mmol) and Pd(dppf)Cl2 (132 mg, 0.18 mmol). The mixture was stirred at 80 C for overnight. Remove the solid by filtration, the filtrate was concentrated and purified by CC (5% to 10% ethyl acetate in petroleum ether) to get 0188-2 (330 mg, 57% yield) as a white solid.
 

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