Home Cart Sign in  
Chemical Structure| 1313509-47-5 Chemical Structure| 1313509-47-5

Structure of 1313509-47-5

Chemical Structure| 1313509-47-5

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1313509-47-5 ]

CAS No. :1313509-47-5
Formula : C31H43NO2
M.W : 461.68
SMILES Code : O=CC1=CC(N(C(CCCCCCCC)CCCCCCCC)C2=C3C=CC(C=O)=C2)=C3C=C1
MDL No. :N/A

Safety of [ 1313509-47-5 ]

Application In Synthesis of [ 1313509-47-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1313509-47-5 ]

[ 1313509-47-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 955964-73-5 ]
  • [ 68-12-2 ]
  • [ 1313509-47-5 ]
YieldReaction ConditionsOperation in experiment
82% 9-Heptadecanyl-2,7-diformylcarbazole (10): 9-Heptadecanyl-2,7-dibromocarbazole (3 g, 5.3 mmol) was solubilized in 130 mL of dry THF and was cooled at -78 °C. Then 16 mL (25.6 mmol) of a solution of n-butyl lithium was added dropwise. The reaction mixture was then heated up at 0 °C for 1 h and cooled down again at -78 °C. Then 6 mL of DMF was added and the reaction was mixed during 4 h at room temperature. The reaction mixture was then poured into 100 mL of cold and lightly acid water, filtered and washed with water. The crude yellow solid was then purified by flash chromatography two times, first in toluene and a second time in a mixture of heptane and ethyl acetate (80/20) to afford a yellow powder (yield: 82percent). 1H NMR (400 MHz, CDCl3): delta (ppm) 10.17 (s, 2H); 8.25 (s, 2H); 8.00 (d, J = 48.1 Hz, 2H); 7.72 (d, J = 8.0 Hz, 2H), 4.68 (tt, J = 10.2, 5.1 Hz, 1H); 2.25 (m, 2H); 1.92 (m, 2H) 1.26-1.09 (m, 28H); 0.80 (t, J = 7.0 Hz, 6H). 13C NMR (101 MHz, CDCl3): delta (ppm) 192.56; 121.28; 113.32; 112.66; 103.47; 57.28; 33.94; 31.83; 29.40; 29.38; 29.19; 26.94; 22.69; 14.16. FT-IR (ATR): nu = 2916, 2844, 1689, 1570, 1460, 1444, 1223, 1166, 992, 856, 803, 731 cm-1. HRMS (EI+, m/z) [M]+ calculated (percent) for C31H43NO2: 461.32938, found 461.32967.
 

Historical Records