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Chemical Structure| 129993-47-1 Chemical Structure| 129993-47-1

Structure of 129993-47-1

Chemical Structure| 129993-47-1

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Product Details of [ 129993-47-1 ]

CAS No. :129993-47-1
Formula : C5H7N3O
M.W : 125.13
SMILES Code : C[N]1C=C(N=C1)C(=O)N
MDL No. :MFCD11054183
InChI Key :AWDCMXSTPBEJMX-UHFFFAOYSA-N
Pubchem ID :14532663

Safety of [ 129993-47-1 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H315-H319-H332-H335
Precautionary Statements:P261-P280-P305+P351+P338

Application In Synthesis of [ 129993-47-1 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 129993-47-1 ]

[ 129993-47-1 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 41716-18-1 ]
  • [ 129993-47-1 ]
YieldReaction ConditionsOperation in experiment
48% To a solution of <strong>[41716-18-1]1-<strong>[41716-18-1]methyl-1H-imidazole-4-carboxylic acid</strong></strong> (1 g, 7.94 mmol) in DCM (10 mL) was added (COd)2 (2 g, 15.9 mmol) and DIVIF (2 drops). After stirred at room temperature for 5 hrs, the reaction mixture was evaporated in vacuum. The residue was then dissloved in 7 N NH3 in MeOH (10 mL). After stirred at room temperature overnight, the reaction mixture was evaporated in vacuum. The residue was purified by flash column chromatograph (ACN in water, 5percent to 60percent) to afford <strong>[41716-18-1]1-<strong>[41716-18-1]methyl-1H-imidazole-4-carboxylic acid</strong></strong> amide (480 mg, 48percent) as a white solid. ?H NIVIR (400 IVIHz, DMSO-d6): oe = 7.62 (d, J= 11.6Hz, 2H), 7.24 (s, 1H), 7.03 (s, 1H), 3.68 (s, 3H).
 

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