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Chemical Structure| 1255789-24-2 Chemical Structure| 1255789-24-2

Structure of 1255789-24-2

Chemical Structure| 1255789-24-2

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Product Details of [ 1255789-24-2 ]

CAS No. :1255789-24-2
Formula : C7H9ClN2O
M.W : 172.61
SMILES Code : NC1=CC(Cl)=CC(OC)=C1N

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Application In Synthesis of [ 1255789-24-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1255789-24-2 ]

[ 1255789-24-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 859877-49-9 ]
  • [ 1255789-24-2 ]
YieldReaction ConditionsOperation in experiment
93% With iron; ammonium chloride; In ethanol; water; for 4h;Reflux; Step 3. 5-Chloro-3-meihoxybenzene-l,2-diamine. A mixture of 4-chloro-2- methoxy-6-nitroaniline (1.01 g, 5 mmol), Fe (1.68 g, 30 mmol), and NH4CI (2.67g, 50 mmol) in EtOH (10 mL) and water (5 mL) was stirred at reflux for 4hr and then filtered. The filtrate was concentrated under reduced pressure and the residue was purified by column chromatography to give 5-chloro-3-methoxybenzene-l,2-diamine (0.80 g, 93% yield) as brown solid. LC-MS: m/z 173 (M+H)+.
 

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