Home Cart Sign in  
Chemical Structure| 1252672-84-6 Chemical Structure| 1252672-84-6

Structure of 1252672-84-6

Chemical Structure| 1252672-84-6

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1252672-84-6 ]

CAS No. :1252672-84-6
Formula : C13H23NO3
M.W : 241.33
SMILES Code : O=C(OC(C)(C)C)NC1(CC2)CCC2(O)CC1
MDL No. :MFCD28403233
InChI Key :MSWXCWNGGPGPDD-UHFFFAOYSA-N
Pubchem ID :91175313

Safety of [ 1252672-84-6 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302
Precautionary Statements:P264-P270-P301+P312-P330

Application In Synthesis of [ 1252672-84-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1252672-84-6 ]

[ 1252672-84-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1127-13-5 ]
  • [ 75-65-0 ]
  • [ 1252672-84-6 ]
YieldReaction ConditionsOperation in experiment
With diphenyl phosphoryl azide; triethylamine; In 1,4-dioxane; at 80℃; Preparation of Bicyclic Amine Intermediate 21 (BAI-21) tent-butyl (4-hydroxybicyclo[2.2.2]oct-1-yl)carbamateTo a solution of <strong>[1127-13-5]4-hydroxybicyclo[2.2.2]octane-1-carboxylic acid</strong> (BAI-20, 340 mg, 2 mol) in dioxane (5 mL) was added triethylamine (202 m g, 2 mmol), diphenyl phosphoryl azide (550 mg, 2 mmol) and tent-butanol (3 g, 40 mmol). The reaction mixture was stirred for 45 minutes at 80 C. overnight. Then the mixture was concentrated under reduced pressure. The residue was dissolved in 30 mL of ethyl acetate and then washed with saturated NaHCO3 and brine. The organic layer was dried over anhydrous Na2SO4 and concentrated to afford the crude titled compound which was used in the next step without further purification.
 

Historical Records

Technical Information

Categories