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Chemical Structure| 1246891-52-0 Chemical Structure| 1246891-52-0

Structure of 1246891-52-0

Chemical Structure| 1246891-52-0

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Product Details of [ 1246891-52-0 ]

CAS No. :1246891-52-0
Formula : C5H13NO2
M.W : 119.16
SMILES Code : C[C@@H](OC)[C@H](N)CO
MDL No. :MFCD19215855

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Application In Synthesis of [ 1246891-52-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1246891-52-0 ]

[ 1246891-52-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 4144-02-9 ]
  • [ 1246891-52-0 ]
YieldReaction ConditionsOperation in experiment
With diborane; In tetrahydrofuran; at 20 - 30℃; for 12.0h; A solution of <strong>[4144-02-9](2S,3R)-2-amino-3-methoxybutanoic acid</strong> (1 g, 7.51 mmol, 1 equiv), diborane hydrogen (15.0 mL, 1 mol/L, 2 equiv) in THF (15 mL) was stirred for 12 h at RT. The reaction was quenched by the addition of 15 mL of methanol. The resulting mixture was diluted with 15 mL of water and washed with 2*30 ml of DCM. The organic layers were combined and dried over Na2SO4. The resulting mixture was concentrated to afford 2.2 g (crude) of the title compound as colorless oil. LCMS (ESI, m/z): 120.09 [M+H]+
 

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