There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.
Type | HazMat fee for 500 gram (Estimated) |
Excepted Quantity | USD 0.00 |
Limited Quantity | USD 15-60 |
Inaccessible (Haz class 6.1), Domestic | USD 80+ |
Inaccessible (Haz class 6.1), International | USD 150+ |
Accessible (Haz class 3, 4, 5 or 8), Domestic | USD 100+ |
Accessible (Haz class 3, 4, 5 or 8), International | USD 200+ |
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CAS No. : | 122632-07-9 | MDL No. : | MFCD24472025 |
Formula : | C11H24N2O2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | FKJWKSFJVZBEEB-UHFFFAOYSA-N |
M.W : | 216.32 | Pubchem ID : | 14185780 |
Synonyms : |
|
Signal Word: | Danger | Class: | 8 |
Precautionary Statements: | P261-P264-P271-P280-P302+P352-P304+P340-P305+P351+P338-P310-P332+P313-P362-P403+P233-P405-P501 | UN#: | 1760 |
Hazard Statements: | H315-H318-H335 | Packing Group: | Ⅲ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
58% | With potassium fluoride; Celite In acetonitrile at 82℃; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: 58 percent / KF, celite / acetonitrile / 82 °C 2: 87 percent / NH2NH2 / methanol / 50 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 4 steps 1: 58 percent / KF, celite / acetonitrile / 82 °C 2: 87 percent / NH2NH2 / methanol / 50 °C 3: 85 percent / CH2Cl2 4: 100 percent / TFA |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 6 steps 1: 58 percent / KF, celite / acetonitrile / 82 °C 2: 87 percent / NH2NH2 / methanol / 50 °C 3: 85 percent / CH2Cl2 4: 100 percent / TFA 5: 65 percent / Na2CO3 / dimethylformamide 6: TFA |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 3 steps 1: 58 percent / KF, celite / acetonitrile / 82 °C 2: 87 percent / NH2NH2 / methanol / 50 °C 3: 85 percent / CH2Cl2 |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 5 steps 1: 58 percent / KF, celite / acetonitrile / 82 °C 2: 87 percent / NH2NH2 / methanol / 50 °C 3: 85 percent / CH2Cl2 4: 100 percent / TFA 5: 65 percent / Na2CO3 / dimethylformamide |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 8 steps 1: 58 percent / KF, celite / acetonitrile / 82 °C 2: 87 percent / NH2NH2 / methanol / 50 °C 3: 85 percent / CH2Cl2 4: 100 percent / TFA 5: 65 percent / Na2CO3 / dimethylformamide 6: TFA 7: TEA / CH2Cl2 8: TFA |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 7 steps 1: 58 percent / KF, celite / acetonitrile / 82 °C 2: 87 percent / NH2NH2 / methanol / 50 °C 3: 85 percent / CH2Cl2 4: 100 percent / TFA 5: 65 percent / Na2CO3 / dimethylformamide 6: TFA 7: TEA / CH2Cl2 |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 9 steps 1: 58 percent / KF, celite / acetonitrile / 82 °C 2: 87 percent / NH2NH2 / methanol / 50 °C 3: 85 percent / CH2Cl2 4: 100 percent / TFA 5: 65 percent / Na2CO3 / dimethylformamide 6: TFA 7: TEA / CH2Cl2 8: TFA 9: DCC, HOBt / CH2Cl2 |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 10 steps 1: 58 percent / KF, celite / acetonitrile / 82 °C 2: 87 percent / NH2NH2 / methanol / 50 °C 3: 85 percent / CH2Cl2 4: 100 percent / TFA 5: 65 percent / Na2CO3 / dimethylformamide 6: TFA 7: TEA / CH2Cl2 8: TFA 9: DCC, HOBt / CH2Cl2 10: Hydrogen / Pd(OH)2 / acetic acid |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux 2: toluene / 20 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With lithium aluminium tetrahydride In tetrahydrofuran at 0℃; Reflux; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 3 steps 1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Reflux 2: toluene / 20 °C 3: 1,3,4,6,7,8-hexahydro-2H-pyrimido[1,2-a]pyrimidine / 20 °C |