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Chemical Structure| 1221567-17-4 Chemical Structure| 1221567-17-4

Structure of 1221567-17-4

Chemical Structure| 1221567-17-4

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Product Details of [ 1221567-17-4 ]

CAS No. :1221567-17-4
Formula : C5H6Cl2N2
M.W : 165.02
SMILES Code : CC1=CN=CN=C1Cl.[H]Cl
MDL No. :MFCD18432626

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Application In Synthesis of [ 1221567-17-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1221567-17-4 ]

[ 1221567-17-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 17758-52-0 ]
  • [ 1221567-17-4 ]
YieldReaction ConditionsOperation in experiment
With trichlorophosphate; at 90.0℃; for 2.5h; A mixture of 5-methyl-3/-/-pyrimidin-4-one (0.60 g, 3.6 mmol) and phosphorous oxychloride (2.0 ml.) was heated at 90 0C for 2.5 h. The mixture was evaporated to dryness under reduced pressure and the resultant solid was purified by sublimation under reduced pressure to furnish the title compound as a white solid. This compound was unstable to air and was used immediately in the next step.
 

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