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Chemical Structure| 119646-69-4 Chemical Structure| 119646-69-4

Structure of 119646-69-4

Chemical Structure| 119646-69-4

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Product Details of [ 119646-69-4 ]

CAS No. :119646-69-4
Formula : C8H13ClN6O
M.W : 244.68
SMILES Code : O=C(C1=NC(Cl)=C(N)N=C1N)NCCNC

Safety of [ 119646-69-4 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H301-H311-H331
Precautionary Statements:P261-P264-P270-P271-P280-P302+P352-P304+P340-P310-P330-P361-P403+P233-P405-P501
Class:6.1
UN#:2811
Packing Group:

Application In Synthesis of [ 119646-69-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 119646-69-4 ]

[ 119646-69-4 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 1458-01-1 ]
  • [ 109-81-9 ]
  • [ 119646-69-4 ]
YieldReaction ConditionsOperation in experiment
In tetrahydrofuran; (1) A mixture of 20 g (99.0 mmol) of methyl 3,5-diamino-6-chloropyrazine-2-carboxylate (see U.S. Pat. No. 4,029,816 for an example of how to obtain this material) and 17 g (230.0 mmol) of N-methylethylenediamine was heated at reflux under an inert atmosphere for 30 hours. The rection mixture was cooled to ambient temperature and the solid was dissolved in 100 ml of tetrahydrofuran. The solution was filtered and evaporated. The residue was crystallized from 2-propanol. There was obtained 15.0 g (61.2 mmol, 61percent) of 3,5-diamino-6-chloro-N-(2-methylaminoethyl)pyrazine-2-carboxamide; mp 142.5°-143° C. Analysis calculated for; C8 H13 ClN6 O: C, 39.27; H, 5.35; N, 34.35; Found: C, 39.28; H, 5.26; N, 34.55.
 

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