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Chemical Structure| 114686-81-6 Chemical Structure| 114686-81-6

Structure of 114686-81-6

Chemical Structure| 114686-81-6

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Product Details of [ 114686-81-6 ]

CAS No. :114686-81-6
Formula : C8H6Cl2O
M.W : 189.04
SMILES Code : O=CCC1=CC=CC(Cl)=C1Cl
MDL No. :MFCD08703372

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Application In Synthesis of [ 114686-81-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 114686-81-6 ]

[ 114686-81-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 114686-85-0 ]
  • [ 114686-81-6 ]
YieldReaction ConditionsOperation in experiment
With sodium hydrogencarbonate; Dess-Martin periodane; In dichloromethane; water; for 1h; A mixture of <strong>[114686-85-0]2-(2,3-dichlorophenyl)ethanol</strong> (0.50 g), NaHCO3 (0.438 g) and Dess-Martin periodinane (1.22 g) in dichloromethane (10 mL) and water (46 mL) was stirred for 1 hour. The mixture was quenched with aqueous NaHCO3 and saturated aqueous Na2S2O3 and extracted with dichloromethane. The extract was dried (Na2SO4), filtered and concentrated. The concentrate was purified on silica gel with an Intelliflash-280 purification system with hexanes/ethyl acetate.
 

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