Home Cart Sign in  
HazMat Fee +

There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.

Type HazMat fee for 500 gram (Estimated)
Excepted Quantity USD 0.00
Limited Quantity USD 15-60
Inaccessible (Haz class 6.1), Domestic USD 80+
Inaccessible (Haz class 6.1), International USD 150+
Accessible (Haz class 3, 4, 5 or 8), Domestic USD 100+
Accessible (Haz class 3, 4, 5 or 8), International USD 200+
Chemical Structure| 1135283-53-2 Chemical Structure| 1135283-53-2

Structure of 1135283-53-2

Chemical Structure| 1135283-53-2

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1135283-53-2 ]

CAS No. :1135283-53-2
Formula : C9H5F3N2O
M.W : 214.14
SMILES Code : O=CC1=CNC2=NC=C(C(F)(F)F)C=C21
MDL No. :MFCD11841013

Safety of [ 1135283-53-2 ]

GHS Pictogram:
Signal Word:Danger
Hazard Statements:H301-H319
Precautionary Statements:P301+P310-P305+P351+P338
Class:6.1
UN#:2811
Packing Group:

Application In Synthesis of [ 1135283-53-2 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1135283-53-2 ]

[ 1135283-53-2 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 1036027-54-9 ]
  • [ 100-97-0 ]
  • [ 1135283-53-2 ]
YieldReaction ConditionsOperation in experiment
With water; acetic acid; for 2.5h;Reflux; b) <strong>[1036027-54-9]5-trifluoromethyl-1H-pyrrolo[2,3-b]pyridine</strong>-3-carbaldehyde can be prepared as follows: Add 926 mg of 1,3,5,7-tetraazatricyclo[3.3.1.1~3,7~]decane to a mixture of 820 mg of <strong>[1036027-54-9]5-trifluoromethyl-1H-pyrrolo[2,3-b]pyridine</strong> in 6 cm3 of water and 3 cm3 of acid acetic. Reflux the reaction mixture for two hours and thirty minutes. Then add 6 cm3 of water to the hot mixture. On returning to a temperature close to 25 C., the mixture is extracted with ethyl acetate (40 cm3). The organic phase is washed with a saturated solution of sodium chloride, dried over magnesium sulphate and concentrated under vacuum. The residue is purified by chromatography on silica (elution with a 20-100% gradient of ethyl acetate in heptane) to obtain 123 mg of <strong>[1036027-54-9]5-trifluoromethyl-1H-pyrrolo[2,3-b]pyridine</strong>-3-carbaldehyde in the form of a beige powder with the following characteristics: LC-MS: retention time 3.14 min; 215(+)=(M+H)(+). 1H-NMR spectrum at 400 MHz: 8.67 (d, J=2.4 Hz, 1H); 8.75 (d, J=2.4 Hz, 1H); 8.69 (s, 1H); 10.00 (s, 1H); 13.17 (s broad, 1H).
 

Historical Records

Technical Information

Categories