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Chemical Structure| 113075-74-4 Chemical Structure| 113075-74-4

Structure of 113075-74-4

Chemical Structure| 113075-74-4

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Product Details of [ 113075-74-4 ]

CAS No. :113075-74-4
Formula : C10H11ClO
M.W : 182.65
SMILES Code : OC1CCCC2=C1C=CC=C2Cl
MDL No. :MFCD16037864

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Application In Synthesis of [ 113075-74-4 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 113075-74-4 ]

[ 113075-74-4 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 26673-30-3 ]
  • [ 113075-74-4 ]
YieldReaction ConditionsOperation in experiment
With hydrogenchloride; sodium borohydrid; (a) 20.6 g of <strong>[26673-30-3]5-chloro-1-tetralone</strong> were dissolved in 100 ml of alcohol, whereupon 2.2 g of sodium borohydride were added portionwise. The reaction mixture was stirred at 40 for 2 hours, then cooled and thereupon treated at room temperature with 32 ml of 2N hydrochloric acid. The mixture was then concentrated in vacuo and extracted with methylene chloride. The organic phases were dried over sodium sulphate and evaporated. The 5-chloro-1-tetralol which remains behind as the residue was processed directly as the crude product.
 

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