Home Cart Sign in  
Chemical Structure| 112755-94-9 Chemical Structure| 112755-94-9

Structure of 112755-94-9

Chemical Structure| 112755-94-9

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 112755-94-9 ]

CAS No. :112755-94-9
Formula : C13H20O3
M.W : 224.30
SMILES Code : O=C1CC2CC3(CC2C1)OCC(C)(C)CO3

Safety of [ 112755-94-9 ]

Application In Synthesis of [ 112755-94-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 112755-94-9 ]

[ 112755-94-9 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 51716-63-3 ]
  • [ 126-30-7 ]
  • [ 112755-94-9 ]
YieldReaction ConditionsOperation in experiment
66% With pyridinium p-toluenesulfonate; In toluene;Dean-Stark; Reflux; Inert atmosphere; To a solution of <strong>[51716-63-3](3as,6as)-tetrahydropentalene-2,5(1H,3H)-dione</strong> (15 g, 108.57 mmol) in toluene (150 mL) was added 2, 2-dimethylpropane-1,3-diol (11.31 g, 108.57 mmol), followed by the addition of PPTS (250 mg) at rt. The reaction mixture was refluxed overnight with a Dean-Stark trap under N 2 atmosphere. After cooled to rt, the reaction mixture was concentrated under vacuum to remove the volatile. The residue was purified by silica gel flash column chromatography (PE: EtOAc = 20: 1) to give the title compound (16 g, yield: 66%) as a white solid.
 

Historical Records