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Chemical Structure| 112089-59-5 Chemical Structure| 112089-59-5

Structure of 112089-59-5

Chemical Structure| 112089-59-5

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Product Details of [ 112089-59-5 ]

CAS No. :112089-59-5
Formula : C11H8N2O4
M.W : 232.19
SMILES Code : O=C(C1=NC2=CC=C([N+]([O-])=O)C=C2C=C1)OC
MDL No. :MFCD08436463

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Application In Synthesis of [ 112089-59-5 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 112089-59-5 ]

[ 112089-59-5 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 67-56-1 ]
  • [ 30836-96-5 ]
  • [ 112089-59-5 ]
YieldReaction ConditionsOperation in experiment
With thionyl chloride; at 25.0℃; for 12h;Cooling with ice; To the reactor, add 6-nitroquinoline-2-carboxylic acid crude product 22g and 150mL methanol, ice bath drops add 23mL thionyl chloride, drip to 25 C stirred for 12 hours. 300mL of water was added to quench the reaction, and after the methanol was removed, the ethyl acetate 3×300mL of the extract was extracted, and the organic phase was washed three times with saturated sodium bicarbonate aqueous solution, and the water and saturated saline were washed three times each. After drying and filtering, spin dry to obtain 23g of reddish-brown solid crude.
 

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