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Chemical Structure| 1082066-01-0 Chemical Structure| 1082066-01-0

Structure of 1082066-01-0

Chemical Structure| 1082066-01-0

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Product Details of [ 1082066-01-0 ]

CAS No. :1082066-01-0
Formula : C7H10N2O2
M.W : 154.17
SMILES Code : O=CC1C=NN(CC(C)O)C=1
MDL No. :N/A

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Application In Synthesis of [ 1082066-01-0 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1082066-01-0 ]

[ 1082066-01-0 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 19686-73-8 ]
  • [ 35344-95-7 ]
  • [ 1082066-01-0 ]
YieldReaction ConditionsOperation in experiment
73% With potassium carbonate; In acetonitrile; at 150℃; for 0.333333h;Microwave irradiation; Preparation 56: Racemic l-(2-Hydroxy-propyl)-l H-<strong>[35344-95-7]pyrazole-4-carbaldehyde</strong>Combine 1 H-<strong>[35344-95-7]pyrazole-4-carbaldehyde</strong> (0.150g, 1.56 mmol), racemic l-bromo-2- propanol (0.26Og, 1.87 mmol), and potassium carbonate (0.323g, 2.34 mmol) in <n="63"/>--62-acetonitrile (2 mL). Heat in microwave at 150 0C for 20 min.. Filter, wash with acetonitrile and concentrate filtrate. Purify via silica gel chromatography, eluting with 0: 100 to 100:0 ethyl acetate:hexanes) to give the title preparation (177 mg, 73percent). GC- MS: m/z = 154 [M+].
 

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