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Chemical Structure| 104174-91-6 Chemical Structure| 104174-91-6

Structure of 104174-91-6

Chemical Structure| 104174-91-6

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Product Details of [ 104174-91-6 ]

CAS No. :104174-91-6
Formula : C11H16O2
M.W : 180.24
SMILES Code : CCCOC1=CC=CC=C1CCO
MDL No. :MFCD14582732

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Application In Synthesis of [ 104174-91-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 104174-91-6 ]

[ 104174-91-6 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 7768-28-7 ]
  • [ 106-94-5 ]
  • [ 104174-91-6 ]
YieldReaction ConditionsOperation in experiment
With sodium hydroxide; sodium chloride; potassium carbonate; In water; acetone; Reference Example 128 A mixture of 2-hydroxyphenethyl alcohol (1.5 g), 1-bromopropane (1.3 ml), potassium carbonate (2.25 g) and acetone (50 ml) was stirred at 60° C. for 64 hours. After concentration under reduced pressure, the residue was mixed with water and was extracted with ethyl acetate. The organic layer was washed with a 1 N aqueous solution of sodium hydroxide and an aqueous saturated solution of sodium chloride, and was dried with magnesium sulfate. The resulting organic layer was concentrated under reduced pressure to obtain 2-propoxyphenethyl alcohol (2.02 g) as a yellow oily substance. 1H-NMR (200 MHz, CDCl3) delta1.06 (3H, t, J=7.5 Hz), 1.68-1.92 (3H, m), 2.93 (2H, t, J=6.4 Hz), 3.81-3.87 (2H, m), 3.95 (2H, t, J=6.4 Hz), 6.84-6.94 (2H, m), 7.15-7.25 (2H, m). IR (neat) 3343, 1601, 1494, 1474, 1454, 1242, 1119, 1049, 1019, 982, 752 cm-1.
 

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