Home Cart Sign in  
Chemical Structure| 1037834-27-7 Chemical Structure| 1037834-27-7

Structure of 1037834-27-7

Chemical Structure| 1037834-27-7

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1037834-27-7 ]

CAS No. :1037834-27-7
Formula : C9H16O3
M.W : 172.22
SMILES Code : O=C(C1CCC(C)(OC)CC1)O
MDL No. :MFCD18375013

Safety of [ 1037834-27-7 ]

GHS Pictogram:
Signal Word:Warning
Hazard Statements:H302-H319
Precautionary Statements:P305+P351+P338

Application In Synthesis of [ 1037834-27-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1037834-27-7 ]

[ 1037834-27-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 67-56-1 ]
  • [ 145576-28-9 ]
  • [ 1037834-27-7 ]
YieldReaction ConditionsOperation in experiment
55% Preparation of 4-Methoxy-4-methylcyclohexanecarboxylic acid; <n="50"/>A suspension of Hg(OAc)2 (2.2 g, 6.96 mmol) in dry methanol (15 mL) was cooled to O0C under stirring, 4-Methylenecyclohexanecarboxylic acid ethyl ester (0.9 g, 5.36 mmol) was added and maintained for 15 min. To the resulted reaction mixture, 3M NaOH (12 mL) was added followed by the addition of a mixture of NaBH4 solution in 3M NaOH solution (12 mL) and maintained for 10 min. The reaction mixture was allowed to rt and maintained for 1h additionally. The reaction mass was filtered through celite bed, the filtrate was cooled, acidified and then was extracted with DCM (100 mL). The organic layer was washed with water (2 x 50 mL), brine solution (50 mL), dried over anhydrous sodium sulfate and concentrated to obtain the crude product. The crude was purified by column chromatography over silica gel column using 10% EtOAc in pet ether as eluting solvent to obtain the pure product (2) as liquid (500 mg, 55%). 1HNMR(CDCl3)-. delta 3.22(s, 1H), 3.15(s, 3H), 2.18-2.36(m, 1H), 1.9(d, 2H)1 1.5-1.82(m, 5H), 1.2-1.32(m, 2H) and 1.1 (s, 3H). Mass: (M-1) 171 calculated for C9H15O3.
 

Historical Records

Technical Information

Categories