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Chemical Structure| 103755-51-7 Chemical Structure| 103755-51-7
Chemical Structure| 103755-51-7

(1-Phenyl-1H-1,2,3-triazol-5-yl)methanol

CAS No.: 103755-51-7

4.5 *For Research Use Only !

Cat. No.: A852529 Purity: 95%

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Product Details of [ 103755-51-7 ]

CAS No. :103755-51-7
Formula : C9H9N3O
M.W : 175.19
SMILES Code : OCC1=CN=NN1C2=CC=CC=C2
MDL No. :MFCD19268877

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Application In Synthesis of [ 103755-51-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 103755-51-7 ]

[ 103755-51-7 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 107-19-7 ]
  • [ 622-37-7 ]
  • [ 103755-58-4 ]
  • [ 103755-51-7 ]
YieldReaction ConditionsOperation in experiment
35% at 90℃; for 2h; EXAMPLE 9: Preparation of jV-((lH-benzo[d]imidazol-2-yl)methyl)-jV-(4-aminobutyl)- 5,6,7,8-tetrahydroquinolin-8-amine tetrahydrochloride (Y).Step a: Preparation of (l-phenyl-lH-l,2,3-triazol-4-yl)methanol (7). Phenyl azide (2.02 g, 17.0 mmol) was dissolved in neat propargyl alcohol (3 mL) and the mixture was heated to 9O0C for 2h. The reaction mixture was cooled to room temperature and the reaction mixture was diluted into diethyl ether and left overnight during which time 7 precipitated as a crystalline solid to afford 1.03 g (35%) of the desired product 7 while the mother liquor contained primarily the regioisomer 9: 1H NMR (400 MHz, CDCl3) delta 7.97, (s, IH), 7.70, (d, J= 8.40 Hz, 2H), 7.50, (m, 2H), 7.41 (m, IH), 4.88, (d, J= 6.00 Hz, 2H), 2.70, (bs, IH).
  • 2
  • [ 62-53-3 ]
  • [ 103755-58-4 ]
  • [ 103755-51-7 ]
 

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