Home Cart Sign in  
Chemical Structure| 1024109-24-7 Chemical Structure| 1024109-24-7

Structure of 1024109-24-7

Chemical Structure| 1024109-24-7

*Storage: {[sel_prStorage]}

*Shipping: {[sel_prShipping]}

,{[proInfo.pro_purity]}

4.5 *For Research Use Only !

{[proInfo.pro_purity]}
Cat. No.: {[proInfo.prAm]} Purity: {[proInfo.pro_purity]}

Change View

Size Price VIP Price

US Stock

Global Stock

In Stock
{[ item.pr_size ]} Inquiry {[ getRatePrice(item.pr_usd,item.pr_rate,item.mem_rate,item.pr_is_large_size_no_price, item.vip_usd) ]}

US Stock: ship in 0-1 business day
Global Stock: ship in 5-7 days

  • {[ item.pr_size ]}

In Stock

- +

Please Login or Create an Account to: See VIP prices and availability

US Stock: ship in 0-1 business day
Global Stock: ship in 2 weeks

  • 1-2 Day Shipping
  • High Quality
  • Technical Support
Product Citations

Alternative Products

Product Details of [ 1024109-24-7 ]

CAS No. :1024109-24-7
Formula : C6H5F3N2
M.W : 162.11
SMILES Code : NNC1=CC(F)=C(F)C=C1F
MDL No. :MFCD17226540

Safety of [ 1024109-24-7 ]

Application In Synthesis of [ 1024109-24-7 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1024109-24-7 ]

[ 1024109-24-7 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 367-34-0 ]
  • [ 1024109-24-7 ]
YieldReaction ConditionsOperation in experiment
67.5% General procedure: Different substituted anilines 3 (10.0mmol) were added to a solution of hydrochloric acid (15mL, 3?4mol L?1), and then sodium nitrite (0.76g, 10.5mmol) dissolving in water (3mL) was dropwise added at 0°C. After 0.5h, tin (II) chloride (4.5g, 20mmol) in 10mL of concentrated hydrochloric acid was dropwise added to the above mixture. The reaction was vigorously stirred for 2h at 0°C, and then was filtered and washed with 3?4molL?1 hydrochloric acid. The precipitate was dissolved in water and filtered. The filtrate was adjusted to pH 12, and the generated solid was collected and dried to afford different substituted phenylhydrazine 4a?k.
 

Historical Records