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Chemical Structure| 102308-68-9 Chemical Structure| 102308-68-9

Structure of 102308-68-9

Chemical Structure| 102308-68-9

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Product Details of [ 102308-68-9 ]

CAS No. :102308-68-9
Formula : C9H10N2O
M.W : 162.19
SMILES Code : O=C1NC2=C(C)C=C(C)C=C2N1

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Application In Synthesis of [ 102308-68-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 102308-68-9 ]

[ 102308-68-9 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 75-44-5 ]
  • [ 3171-46-8 ]
  • [ 102308-68-9 ]
  • 2
  • [ 32315-10-9 ]
  • [ 3171-46-8 ]
  • [ 102308-68-9 ]
YieldReaction ConditionsOperation in experiment
In acetonitrile; for 1.0h; A mixture of 4,6-dimethyl-2-nitroaniline (10.0 g, 60.2 mmol) and 10% Pd/C (1.0 g) in EtOH (300 niL) was stirred under an atmosphere of hydrogen (ca. 1 atm) for 3 h, then filtered through a Celite pad and concentrated in vacuo. The crude solid was dissolved in CH3CN (200 mL) and triphosgene (15.0 g, 50.5 mmol) was added. The mixture was stirred for 1 h, then H2O (200 mL) was added slowly and stirring was continued for 1 h. The precipitate was isolated by filtration and dried to give the title compound. MS: mlz = 163 (M + 1).
 

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