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Chemical Structure| 102243-12-9 Chemical Structure| 102243-12-9

Structure of 102243-12-9

Chemical Structure| 102243-12-9

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Product Details of [ 102243-12-9 ]

CAS No. :102243-12-9
Formula : C12H13N3S
M.W : 231.32
SMILES Code : CC1=CC(C)=NC(SC2=CC=C(N)C=C2)=N1
MDL No. :MFCD00203030

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Application In Synthesis of [ 102243-12-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 102243-12-9 ]

[ 102243-12-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 35144-22-0 ]
  • [ 1193-02-8 ]
  • [ 102243-12-9 ]
YieldReaction ConditionsOperation in experiment
75% With potassium carbonate; In N,N-dimethyl-formamide; at 100℃; for 2h; General procerure: A solution of <strong>[35144-22-0]4,6-dimethyl-2-(methylsulfonyl)pyrimidine</strong> (18 mmol), 4-aminophenol or 4-aminobenzenethiol (18 mmol) and K2CO3 (36 mmol) in DMF (50 mL) was stirred at 100 C for 2 h. The reaction mixture was poured into water and extracted with EtOAc. The organic layer was washed with water and saturated brine, dried over Na2SO4 and evaporated. The residue was purified by column chromatography on silica gel (PE:EA = 2:1) to give the compound 3a,3b.
 

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