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[ CAS No. 87184-23-4 ] 2-((tert-Butoxycarbonyl)amino)-3-(3-fluorophenyl)propanoic acid

Cat. No.: A678838
Chemical Structure| 87184-23-4
Chemical Structure| 87184-23-4
 Structure of 87184-23-4
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CAS No. :87184-23-4 MDL No. :MFCD05865250
Formula : C14H18FNO4 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 283.30 Pubchem ID :-
Synonyms :

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* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 87184-23-4 ]

[ 87184-23-4 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 58632-95-4 ]
  • [ 456-88-2 ]
  • [ 87184-23-4 ]
Reference： [1]Journal of Medicinal Chemistry,1983,vol. 26,p. 1725 - 1729
  • 2
  • [ 123-91-1 ]
  • [ 24424-99-5 ]
  • [ 456-88-2 ]
  • [ 87184-23-4 ]
YieldReaction ConditionsOperation in experiment
With sodium carbonate; In water; L-2-tert-Butoxycarbonylamino-3-(3-fluoro-phenyl)-propionic acid A mixture of L-2-amino-3-(3-fluoro-phenyl)-propionic acid (20.0 g, 110 mmol, 1 eq) in H2O (100 mL) was treated with Na2CO3 (16.2 g, 153 mmol, 1.4 eq) in H2O (40 mL) followed by 1,4-dioxane (100 mL) and cooled to 0° C. The BOC2O was added and the reaction mixture was stirred at ambient temperature for 5 h after which the dioxane was evaporated. H2O (125 mL) was then added and the mixture then washed with Et2O (2*100 mL). The aqueous phase was acidified with 10percent citric acid followed by extraction with EtOAc (2*300 mL). The combined EtOAc layers were washed with H2O (2*150 mL), brine (150 mL), dried (Na2SO4) and concentrated to give the acid as a colorless, viscous oil which slowly solidified upon standing (31 g, quant). 1H NMR (CDCl3) 7.33-7.26 (m,1H), 7.00-6.91 (m,3H), 4.96 (s, 1H), 4.62 (bs, 1H), 3.23 (dd, J=14, 5.3, 2H), 1.44 (s, 9H); Anal Calcd for C14H18NO4F: C, 5936; H, 6.40; N, 4.94. Found: C, 59.29; H, 6.34; N, 4.90.
Reference： [1]Patent: US2004/204591,2004,A1

Tags: 87184-23-4 synthesis path| 87184-23-4 SDS| 87184-23-4 COA| 87184-23-4 purity| 87184-23-4 application| 87184-23-4 NMR| 87184-23-4 COA| 87184-23-4 structure

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