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Alternatived Products of [ 24706-47-6 ]
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Product Details of [ 24706-47-6 ]

CAS No. :24706-47-6 MDL No. :MFCD00128477
Formula : C14H16ClNO Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 249.74 Pubchem ID :-
Synonyms :

Safety of [ 24706-47-6 ]

Signal Word: Class:
Precautionary Statements: UN#:
Hazard Statements: Packing Group:

Application In Synthesis of [ 24706-47-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 24706-47-6 ]

[ 24706-47-6 ] Synthesis Path-Downstream   1~2

  • 1
  • [ 17115-51-4 ]
  • [ 24706-47-6 ]
  • [ 456-48-4 ]
  • [ 1265632-11-8 ]
YieldReaction ConditionsOperation in experiment
65% at 90℃; for 12h;Neat (no solvent); Aldehyde 1 (1 mmol), dihydrothiophen-3(2H)-one-1,1-dioxide 2 (0.134 g, 1 mmol), enaminone 3 (1 mmol) and were triturated together in an agate mortar for 5 minutes. Then the mixture was kept at 90 C for a certain time (monitored by TLC). The result mixture was washed with water and recrystallized from ethanol (95 %) to give pure product 4.
Reference： [1]Bioorganic and Medicinal Chemistry Letters,2011,vol. 21,p. 453 - 455
  • 2
  • [ 24706-47-6 ]
  • [ 59046-72-9 ]
  • 3-((4-chlorophenyl)amino)-5,5-dimethyl-2-(3-phenyl-1H-isochromen-1-yl)cyclohex-2-enone [ No CAS ]
YieldReaction ConditionsOperation in experiment
75% With silver nitrate; In N,N-dimethyl acetamide; at 60℃; for 12h;Schlenk technique; General procedure: The substrate <strong>[59046-72-9]2-(phenylethynyl)benzaldehyde</strong> (1a, 0.5 mmol, 0.1030 g), 5,5-dimethyl-3-(phenylamino)cyclohex-2-enone (2a, 1.0 mmol, 0.2151 g, 2 equiv) and AgNO3 (0.05 mmol, 0.0085 g, 10 mol %) were added to a 25 mL Schlenk tube, followed by addition of dry DMA (2.0 mL). The mixture was stirred at 60 C for 12 h. The solution was then quenched by H2O and extracted with EtOAc, the combined organic layers were dried over Na2SO4, filtered, and evaporated under vaccum. The residue was purified by column chromatography on silica gel (eluent: light petroleum ether: ethyl acetate, V: V = 5: 1) to afford the desired product 5,5-dimethyl-2-(3-phenyl-1H-isochromen-1-yl)-3-(phenylamino)cyclohex-2-enone (3a).
Reference： [1]Tetrahedron,2017,vol. 73,p. 5731 - 5737

Tags: 24706-47-6 synthesis path| 24706-47-6 SDS| 24706-47-6 COA| 24706-47-6 purity| 24706-47-6 application| 24706-47-6 NMR| 24706-47-6 COA| 24706-47-6 structure

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