There will be a HazMat fee per item when shipping a dangerous goods. The HazMat fee will be charged to your UPS/DHL/FedEx collect account or added to the invoice unless the package is shipped via Ground service. Ship by air in Excepted Quantity (each bottle), which is up to 1g/1mL for class 6.1 packing group I or II, and up to 25g/25ml for all other HazMat items.
Type | HazMat fee for 500 gram (Estimated) |
Excepted Quantity | USD 0.00 |
Limited Quantity | USD 15-60 |
Inaccessible (Haz class 6.1), Domestic | USD 80+ |
Inaccessible (Haz class 6.1), International | USD 150+ |
Accessible (Haz class 3, 4, 5 or 8), Domestic | USD 100+ |
Accessible (Haz class 3, 4, 5 or 8), International | USD 200+ |
CAS No. : | 21254-22-8 | MDL No. : | MFCD12405952 |
Formula : | C8H8Cl2N4 | Boiling Point : | No data available |
Linear Structure Formula : | - | InChI Key : | SHTPXXJWYCEZPN-UHFFFAOYSA-N |
M.W : | 231.08 | Pubchem ID : | 42609352 |
Synonyms : |
Signal Word: | Danger | Class: | 6.1 |
Precautionary Statements: | P261-P264-P270-P271-P280-P302+P352-P304+P340-P310-P330-P361-P403+P233-P405-P501 | UN#: | 2811 |
Hazard Statements: | H301-H311-H331 | Packing Group: | Ⅲ |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With triethylamine; In tetrahydrofuran; at 50℃; | A solution of 4,6-dichloro-1-isopropyl-1H-pyrazolo[3,4-djpyrimidine (54 mg, 0.234 mmol) and TEA(100 tL, 0.72 mmol) in 1 mL THF was prepared. 1-[4-(Trifluoromethyl)phenyljethan-1-amine (88mg, 0.468 mmol) was then added to the reaction mixture and it was stirred overnight at 50 C on aheating block. The next day, the reaction mixture was transferred to a l3xlOOmm test tube, and theTHF was removed under a stream of nitrogen. The crude residue was then dissolved in DMSO (1 mL)and purified by mass-directed HPLC (2 cm x 5cm C18, acetonitrile-water gradient, 0.05% NH4OHadded) to afford the product as a solid. LC-MS (+ESI) m/z = 384.4 and 386.3 (M+2+H)t |
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