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CAS No. : | 157864-32-9 | MDL No. : | MFCD03691634 |
Formula : | C15H12ClN3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 269.73 | Pubchem ID : | - |
Synonyms : |
Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
59% | With hydrogenchloride; In water; isopropyl alcohol; at 90℃;Sealed tube; | General procedure: A solution of intermediate (1.0 equiv.) in isopropanol, 1M hydrochloric acid (1.2 equiv.) and aniline (1.2 equiv.) were added. The reaction stirred at 90oC overnight in a sealed tube. Filtration and washed the resultant by cooled isopropanol, dried under vacuum. The solid was collected |
22.4% | With hydrogenchloride; In water; isopropyl alcohol; at 90℃;Sealed tube; | General procedure: A solution of intermediate 0.10 g (1.0 equiv.), aniline 1.2 equiv in isopropanol in a sealed tube and 1M hydrochloric acid 1.2 equiv were added. The reaction stirred at 90C overnight. Filtered and washed the crystallized by cold isopropanol,dried under vacuum. The solid was collected to yield a product . |