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[ CAS No. 362703-35-3 ] 1-tert-Butyl 4-methyl 4-(aminomethyl)piperidine-1,4-dicarboxylate

Cat. No.: A864520
Chemical Structure| 362703-35-3
Chemical Structure| 362703-35-3
 Structure of 362703-35-3 * Storage: Keep in dark place,Sealed in dry,2-8°C
Purity Size Price USA Stock *0-1 Day Global Stock *5-7 Days Quantity
98% 250mg $133.00 Inquiry 1-2 weeks
98% 1g $406.00 Inquiry 1-2 weeks

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* Storage: Keep in dark place,Sealed in dry,2-8°C

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For Research Only 120K+ Compounds Competitive Price 1-2 Day Shipping

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COA NMR CNMR HPLC LC-MS

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Product Details of [ 362703-35-3 ]

CAS No. :362703-35-3 MDL No. :MFCD07784122
Formula : C13H24N2O4 Boiling Point : -
Linear Structure Formula :- InChI Key :-
M.W : 272.34 Pubchem ID :-
Synonyms :

Safety of [ 362703-35-3 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 362703-35-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 362703-35-3 ]

[ 362703-35-3 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 362703-34-2 ]
  • [ 362703-35-3 ]
YieldReaction ConditionsOperation in experiment
81% With hydrogen;platinum(IV) oxide; In ethyl acetate; under 2585.81 Torr; for 2.0h; A solution of the piperidine (1.07 g, 3.98 mmol) from reaction (24b) and a catalytic amount of platinum oxide in acetic acid (20 mL) was pressurized with 50 psi of hydrogen for 2 hr. The mixture was filtered through Celite and concentrated. The residue was dissolved in ethyl acetate (20 mL) and washed with saturated sodium bicarbonate solution (2×20mL) and brine (2×20 mL). The organic layer was dried and concentrated to give the desired amine (880 mg, 81%). MS found: (M+H)+=273.
60% With hydrogen; nickel; triethylamine; In methanol; under 2068.65 Torr; To a solution of intermediate 3 (10 g, 37.3 mmol) and triethylamine (1 mL) in MeOH (200 mL) was added Raney-Ni carefully. The resulting mixture was hydrogenated (40 psi H2) overnight. The reaction was filtered through celite, concentrated under vacuum, and purified by preparative HPLC to give intermediate 4 (6 g, 60% yield) as a colorless oil.
Reference： [1]Patent: US2004/72802,2004,A1 .Location in patent: Page/Page column 47
[2]Bioorganic and Medicinal Chemistry Letters,2011,vol. 21,p. 5910 - 5915
[3]Patent: WO2015/150337,2015,A1 .Location in patent: Page/Page column 34; 35
[4]Bioorganic and Medicinal Chemistry Letters,2006,vol. 16,p. 2699 - 2704

Tags: 362703-35-3 synthesis path| 362703-35-3 SDS| 362703-35-3 COA| 362703-35-3 purity| 362703-35-3 application| 362703-35-3 NMR| 362703-35-3 COA| 362703-35-3 structure

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