[ CAS No. 7255-83-6 ] {[proInfo.proName]}

Name: 7255-83-6|2,2'-([1,1'-Biphenyl]-4,4'-diyl)diacetonitrile|98%
Brand: Ambeed
SKU: A1164720
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Quality Control of [ 7255-83-6 ]

COA NMR CNMR HPLC LC-MS

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SDS Specification

Alternatived Products of [ 7255-83-6 ]

Product Details of [ 7255-83-6 ]

CAS No. :	7255-83-6	MDL No. :	MFCD00051458
Formula :	C₁₆H₁₂N₂	Boiling Point :	-
Linear Structure Formula :	-	InChI Key :	GICPRLWIFVXEPU-UHFFFAOYSA-N
M.W :	232.28	Pubchem ID :	252356
Synonyms :

Safety of [ 7255-83-6 ]

Signal Word:	Danger	Class:	6.1
Precautionary Statements:	P261-P280-P305+P351+P338-P311	UN#:	3439
Hazard Statements:	H302+H312-H315-H319-H331-H335	Packing Group:	Ⅲ
GHS Pictogram:

Application In Synthesis of [ 7255-83-6 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

Downstream synthetic route of [ 7255-83-6 ]

[ 7255-83-6 ] Synthesis Path-Downstream 1~18

1
[ 64-17-5 ]
[ 7255-83-6 ]
[ 57186-86-4 ]

Yield	Reaction Conditions	Operation in experiment
	With sulfuric acid

Reference： [1]Current Patent Assignee: EASTMAN KODAK CO - US2789971, 1953, A

2
[ 64-17-5 ]
[ 7255-83-6 ]
2,2'-biphenyl-4,4'-diyl-di-acetamidine; dihydrochloride [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
	With hydrogenchloride Behandeln des Reaktionsprodukts mit aethanol. Ammoniak;

Reference： [1]Hager; Liu [Journal of the American Pharmaceutical Association (1912), 1952, vol. 41, p. 115,117] Ashley et al. [Journal of the Chemical Society, 1942, p. 103,107]

3
[ 1667-10-3 ]
[ 151-50-8 ]
[ 7255-83-6 ]

Yield	Reaction Conditions	Operation in experiment
	With ethanol

Reference： [1]v. Braun; Irmisch; Nelles [Chemische Berichte, 1933, vol. 66, p. 1471,1474]

4
[ 7255-83-6 ]
[ 19806-14-5 ]

Yield	Reaction Conditions	Operation in experiment
92%	With potassium hydroxide In ethanol at 150℃; for 0.0833333h; microwave irradiation;
87%	Stage #1: 4,4’-bis(cyanomethyl)-1,1’biphenyl With sulfuric acid In water for 2h; Reflux; Stage #2: With sodium hydroxide In ethanol; water for 24h; Reflux;	1 Synthesis of 1,1’-biphenyl-4,4’-di(acetic acid) (H₂bpda), 1 Compound B (10.9 g, 47 mmol) was added in small portions to half concentrated sulfuric acid (250 mL) while stirring and then refluxed for 2 h. After cooling to room temperature the suspension was poured in iced water (500 mL) and stirred for 15 min and afterwards filtered and washed with iced water (1 L) and dried in vacuum over night at 323 K. The dry compound was added to a mixture of sodium hydroxide solution (12.8 g, 0.32 mmol NaOH in 100 mL water) and ethanol (175 mL) and refluxed for 24 h. After cooling to room temperature half concentrated hydrochloric solution - was added drop wise to the yellow solution to precipitate an off white solid. The suspension was diluted by addition to iced water (500 mL) and stirred for 15 min. Afterwards the precipitate was filtered and washed with iced water (1 L) and dried in vacuum over night at 323 K to afford compound C (11.1 g, 87 %) as an off white solid. 1H-NMR (200 MHz, DMSO-D6): σ 3.61 (s, 4H, -CH2-), 7.34 & 7.60 (d, 8H, -CH-), 12.36 (s, 2H, -COOH). EI-MS at 150 °C (M = C16H14O4 (270.28) m/z (%) 270 (40) [M], 225 (100) [M - COOH], 211 (35) [M - CH2-COOH], 180 (43) [M - 2x COOH], 152 (19) [M - 2x CH2-COOH].
73%	Stage #1: 4,4’-bis(cyanomethyl)-1,1’biphenyl With potassium hydroxide In ethanol; water Stage #2: With hydrogenchloride In ethanol; water

	With hydrogenchloride at 130℃;
	Stage #1: 4,4’-bis(cyanomethyl)-1,1’biphenyl With potassium hydroxide; ethanol at 150℃; for 0.0833333h; Microwave irradiation; Stage #2: With hydrogenchloride In water

Reference： [1]Morini, Giovanni; Comini, Mara; Rivara, Mirko; Rivara, Silvia; Lorenzi, Simone; Bordi, Fabrizio; Mor, Marco; Flammini, Lisa; Bertoni, Simona; Ballabeni, Vigilio; Barocelli, Elisabetta; Plazzi, Pier Vincenzo [Bioorganic and Medicinal Chemistry Letters, 2006, vol. 16, # 15, p. 4063 - 4067]
[2]Makhloufi, Gamall; Francis, Biju; Dechnik, Janina; Strzelczyk, Alexander; Janiak, Christoph [Polyhedron, 2017, vol. 127, p. 59 - 67]
[3]Masciocchi, Norberto; Galli, Simona; Colombo, Valentina; Maspero, Angelo; Palmisano, Giovanni; Seyyedi, Behnam; Lamberti, Carlo; Bordiga, Silvia [Journal of the American Chemical Society, 2010, vol. 132, # 23, p. 7902 - 7904]
[4]v. Braun; Irmisch; Nelles [Chemische Berichte, 1933, vol. 66, p. 1471,1474]
[5]Location in patent: experimental part Morini, Giovanni; Comini, Mara; Rivara, Mirko; Rivara, Silvia; Bordi, Fabrizio; Plazzi, Pier Vincenzo; Flammini, Lisa; Saccani, Francesca; Bertoni, Simona; Ballabeni, Vigilio; Barocelli, Elisabetta; Mor, Marco [Bioorganic and Medicinal Chemistry, 2008, vol. 16, # 23, p. 9911 - 9924]

5
[ 7255-83-6 ]
[ 30596-04-4 ]

Yield	Reaction Conditions	Operation in experiment
	With sodium hydroxide

Reference： [1]Cavallini; Massarani [Farmaco, Edizione Scientifica, 1953, vol. 8, p. 503,508]

6
[ 7255-83-6 ]
[ 100-52-7 ]
4.4'-bis-(2<i>t</i>-phenyl-1-cyano-vinyl)-biphenyl [ No CAS ]

Reference： [1]v. Braun; Irmisch; Nelles [Chemische Berichte, 1933, vol. 66, p. 1471,1474]

Yield	Reaction Conditions	Operation in experiment
	Biphenyl mit HBr, Paraformaldehyd und NaCN;
	Bis(1,5-Cyclooctadien)Ni, p-Bromphenylacetonitril;
	Entspr. Bis-chlormethyl-diphenyl;

8
[ 1667-10-3 ]
[ 143-33-9 ]
[ 7255-83-6 ]

Reference： [1]Bioorganic and Medicinal Chemistry Letters,2006,vol. 16,p. 4063 - 4067
[2]Bioorganic and Medicinal Chemistry,2008,vol. 16,p. 9911 - 9924

9
[ 7255-83-6 ]
1,1'-[biphenyl-4,4'-diylbis(ethylene)]bis-piperidine [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 3 steps 1.1: 92 percent / KOH / ethanol / 0.08 h / 150 °C / 7500.6 Torr / microwave irradiation 2.1: CDI / tetrahydrofuran / 0.08 h / 130 °C / 7500.6 Torr / microwave irradiation 2.2: 77 percent / tetrahydrofuran / 0.08 h / 130 °C / 7500.6 Torr / microwave irradiation 3.1: 85 percent / RedAl(R) / toluene / 3 h / Heating

10
[ 7255-83-6 ]
[ 855256-71-2 ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 2 steps 1.1: 92 percent / KOH / ethanol / 0.08 h / 150 °C / 7500.6 Torr / microwave irradiation 2.1: CDI / tetrahydrofuran / 0.08 h / 130 °C / 7500.6 Torr / microwave irradiation 2.2: 77 percent / tetrahydrofuran / 0.08 h / 130 °C / 7500.6 Torr / microwave irradiation

11
[ 7255-83-6 ]
[ 4371-13-5 ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 2 steps 1: H₂SO₄ 2: LiAlH₄; diethyl ether

Reference： [1]Current Patent Assignee: EASTMAN KODAK CO - US2789971, 1953, A

12
[ 7255-83-6 ]
biphenyl-4,4'-diyldioxy-di-acetic acid bis-(2-diethylamino-ethyl ester) [ No CAS ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 2 steps 1: aqueous NaOH

Reference： [1]Cavallini; Massarani [Farmaco, Edizione Scientifica, 1953, vol. 8, p. 503,508]

13
[ 92-52-4 ]
[ 7255-83-6 ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 2 steps 1: petroleum ether; HCl; ZnCl₂ / zuletzt unter Erwaermen 2: aqueous ethanol

Reference： [1]v. Braun; Irmisch; Nelles [Chemische Berichte, 1933, vol. 66, p. 1471,1474]

14
[ 7255-83-6 ]
[ 57186-86-4 ]

Yield	Reaction Conditions	Operation in experiment
	Multi-step reaction with 2 steps 1: aqueous hydrochloric acid / 130 °C 2: hydrogen chloride; ethanol

Reference： [1]v. Braun; Irmisch; Nelles [Chemische Berichte, 1933, vol. 66, p. 1471,1474]

15
[ 342-24-5 ]
[ 7255-83-6 ]
[ 1227300-73-3 ]
[ 1227300-74-4 ]

Yield	Reaction Conditions	Operation in experiment
1: 14% 2: 9%	With potassium <i>tert</i>-butylate In N,N-dimethyl-formamide at 100 - 110℃; for 3h;

Reference： [1]Location in patent: experimental part Kim, Sung Hwan; Kim, Se Hee; Kim, Ko Hoon; Kim, Jae Nyoung [Bulletin of the Korean Chemical Society, 2010, vol. 31, # 3, p. 708 - 711]

16
[ 773837-37-9 ]
[ 1667-10-3 ]
[ 7255-83-6 ]

Yield	Reaction Conditions	Operation in experiment
75%	In dimethyl sulfoxide at 40℃; for 8h;

Reference： [1]Masciocchi, Norberto; Galli, Simona; Colombo, Valentina; Maspero, Angelo; Palmisano, Giovanni; Seyyedi, Behnam; Lamberti, Carlo; Bordiga, Silvia [Journal of the American Chemical Society, 2010, vol. 132, # 23, p. 7902 - 7904]

17
[ 773837-37-9 ]
[ 20248-86-6 ]
[ 7255-83-6 ]

Yield	Reaction Conditions	Operation in experiment
	In water for 24h; Reflux;

Reference： [1]Nouri; Abedi; Morsali [RSC Advances, 2016, vol. 6, # 103, p. 101652 - 101659]

18
[ 1667-10-3 ]
[ 7255-83-6 ]

Yield	Reaction Conditions	Operation in experiment
90%	With sodium cyanide; In dimethyl sulfoxide; at 20 - 49.84℃; for 44h;	4,4?-bis(chloromethyl)-1,1?-biphenyl (13.1 g, 52 mmol, 1 eq) A, was added in small portions to a suspension of NaCN (5.35 g, 0.109 mmol, 2.05 eq) in DMSO (50 mL) while stirring. While adding A the suspension will turn pale yellow. After adding of A the mixture was heated under stirring at 323 K for 8 h and afterwards stirred for 36 h at room temperature. The now orange-brown suspension was poured in iced water (500 mL) and a yellow solid precipitated, which was stirred further for 30 min. After filtration and washing with iced water (500 mL) the filter cake was dried over night at 323 C in vacuum to afford the desired intermediate B (10.9 g, 90 %) (1H-NMR (200 MHz, DMSO-D6): sigma 4.08 (s, 2H, -CH2-), 7.44 & 7.71 (d, 8H, -CH-). EI-MS at 100 C (M = C16H12N2 (232.29) m/z (%) 232 (100) [M], 192 (78) [M - CH2-CN], 152 (19) [M - 2x CH2-CN].

Reference： [1]Polyhedron,2017,vol. 127,p. 59 - 67

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P101	If medical advice is needed,have product container or label at hand.
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Code	Phrase
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P234	Keep only in original container.
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Code	Phrase
P301	IF SWALLOWED:
P304	IF INHALED:
P305	IF IN EYES:
P306	IF ON CLOTHING:
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P313	Get medical advice/attention.
P314	Get medical advice/attention if you feel unwell.
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P320
P302 + P352	IF ON SKIN: wash with plenty of soap and water.
P321
P322
P330	Rinse mouth.
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P336	Thaw frosted parts with lukewarm water. Do not rub affected area.
P337	If eye irritation persists:
P338	Remove contact lenses, if present and easy to do. Continue rinsing.
P340	Remove victim to fresh air and keep at rest in a position comfortable for breathing.
P341	If breathing is difficult, remove victim to fresh air and keep at rest in a position comfortable for breathing.
P342	If experiencing respiratory symptoms:
P350	Gently wash with plenty of soap and water.
P351	Rinse cautiously with water for several minutes.
P352	Wash with plenty of soap and water.
P353	Rinse skin with water/shower.
P360	Rinse immediately contaminated clothing and skin with plenty of water before removing clothes.
P361	Remove/Take off immediately all contaminated clothing.
P362	Take off contaminated clothing and wash before reuse.
P363	Wash contaminated clothing before reuse.
P370	In case of fire:
P371	In case of major fire and large quantities:
P372	Explosion risk in case of fire.
P373	DO NOT fight fire when fire reaches explosives.
P374	Fight fire with normal precautions from a reasonable distance.
P376	Stop leak if safe to do so. Oxidising gases (section 2.4) 1
P377	Leaking gas fire: Do not extinguish, unless leak can be stopped safely.
P378
P380	Evacuate area.
P381	Eliminate all ignition sources if safe to do so.
P390	Absorb spillage to prevent material damage.
P391	Collect spillage. Hazardous to the aquatic environment
P301 + P310	IF SWALLOWED: Immediately call a POISON CENTER or doctor/physician.
P301 + P312	IF SWALLOWED: call a POISON CENTER or doctor/physician IF you feel unwell.
P301 + P330 + P331	IF SWALLOWED: Rinse mouth. Do NOT induce vomiting.
P302 + P334	IF ON SKIN: Immerse in cool water/wrap in wet bandages.
P302 + P350	IF ON SKIN: Gently wash with plenty of soap and water.
P303 + P361 + P353	IF ON SKIN (or hair): Remove/Take off Immediately all contaminated clothing. Rinse SKIN with water/shower.
P304 + P312	IF INHALED: Call a POISON CENTER or doctor/physician if you feel unwell.
P304 + P340	IF INHALED: Remove victim to fresh air and Keep at rest in a position comfortable for breathing.
P304 + P341	IF INHALED: If breathing is difficult, remove victim to fresh air and keep at rest in a position comfortable for breathing.
P305 + P351 + P338	IF IN EYES: Rinse cautiously with water for several minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
P306 + P360	IF ON CLOTHING: Rinse Immediately contaminated CLOTHING and SKIN with plenty of water before removing clothes.
P307 + P311	IF exposed: call a POISON CENTER or doctor/physician.
P308 + P313	IF exposed or concerned: Get medical advice/attention.
P309 + P311	IF exposed or if you feel unwell: call a POISON CENTER or doctor/physician.
P332 + P313	IF SKIN irritation occurs: Get medical advice/attention.
P333 + P313	IF SKIN irritation or rash occurs: Get medical advice/attention.
P335 + P334	Brush off loose particles from skin. Immerse in cool water/wrap in wet bandages.
P337 + P313	IF eye irritation persists: Get medical advice/attention.
P342 + P311	IF experiencing respiratory symptoms: call a POISON CENTER or doctor/physician.
P370 + P376	In case of fire: Stop leak if safe to Do so.
P370 + P378	In case of fire:
P370 + P380	In case of fire: Evacuate area.
P370 + P380 + P375	In case of fire: Evacuate area. Fight fire remotely due to the risk of explosion.
P371 + P380 + P375	In case of major fire and large quantities: Evacuate area. Fight fire remotely due to the risk of explosion.
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P401
P402	Store in a dry place.
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Physical hazards
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H200	Unstable explosive
H201	Explosive; mass explosion hazard
H202	Explosive; severe projection hazard
H203	Explosive; fire, blast or projection hazard
H204	Fire or projection hazard
H205	May mass explode in fire
H220	Extremely flammable gas
H221	Flammable gas
H222	Extremely flammable aerosol
H223	Flammable aerosol
H224	Extremely flammable liquid and vapour
H225	Highly flammable liquid and vapour
H226	Flammable liquid and vapour
H227	Combustible liquid
H228	Flammable solid
H229	Pressurized container: may burst if heated
H230	May react explosively even in the absence of air
H231	May react explosively even in the absence of air at elevated pressure and/or temperature
H240	Heating may cause an explosion
H241	Heating may cause a fire or explosion
H242	Heating may cause a fire
H250	Catches fire spontaneously if exposed to air
H251	Self-heating; may catch fire
H252	Self-heating in large quantities; may catch fire
H260	In contact with water releases flammable gases which may ignite spontaneously
H261	In contact with water releases flammable gas
H270	May cause or intensify fire; oxidizer
H271	May cause fire or explosion; strong oxidizer
H272	May intensify fire; oxidizer
H280	Contains gas under pressure; may explode if heated
H281	Contains refrigerated gas; may cause cryogenic burns or injury
H290	May be corrosive to metals
Health hazards
Code	Phrase
H300	Fatal if swallowed
H301	Toxic if swallowed
H302	Harmful if swallowed
H303	May be harmful if swallowed
H304	May be fatal if swallowed and enters airways
H305	May be harmful if swallowed and enters airways
H310	Fatal in contact with skin
H311	Toxic in contact with skin
H312	Harmful in contact with skin
H313	May be harmful in contact with skin
H314	Causes severe skin burns and eye damage
H315	Causes skin irritation
H316	Causes mild skin irritation
H317	May cause an allergic skin reaction
H318	Causes serious eye damage
H319	Causes serious eye irritation
H320	Causes eye irritation
H330	Fatal if inhaled
H331	Toxic if inhaled
H332	Harmful if inhaled
H333	May be harmful if inhaled
H334	May cause allergy or asthma symptoms or breathing difficulties if inhaled
H335	May cause respiratory irritation
H336	May cause drowsiness or dizziness
H340	May cause genetic defects
H341	Suspected of causing genetic defects
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H361d	Suspected of damaging the unborn child
H362	May cause harm to breast-fed children
H370	Causes damage to organs
H371	May cause damage to organs
H372	Causes damage to organs through prolonged or repeated exposure
H373	May cause damage to organs through prolonged or repeated exposure
Environmental hazards
Code	Phrase
H400	Very toxic to aquatic life
H401	Toxic to aquatic life
H402	Harmful to aquatic life
H410	Very toxic to aquatic life with long-lasting effects
H411	Toxic to aquatic life with long-lasting effects
H412	Harmful to aquatic life with long-lasting effects
H413	May cause long-lasting harmful effects to aquatic life
H420	Harms public health and the environment by destroying ozone in the upper atmosphere

[ CAS No. 7255-83-6 ] {[proInfo.proName]}

Quality Control of [ 7255-83-6 ]

Related Doc. of [ 7255-83-6 ]

Product Details of [ 7255-83-6 ]

Safety of [ 7255-83-6 ]

Application In Synthesis of [ 7255-83-6 ]

[ 7255-83-6 ] Synthesis Path-Downstream 1~18

Precautionary Statements-General

Prevention

Response

Storage

Disposal

Physical hazards

Health hazards

Environmental hazards

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