Alternatived Products of [ 60612-00-2 ]
Product Details of [ 60612-00-2 ]
CAS No. : | 60612-00-2 |
MDL No. : | MFCD18762118 |
Formula : |
C10H18O3
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | - |
M.W : |
186.25
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Pubchem ID : | - |
Synonyms : |
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Safety of [ 60612-00-2 ]
Signal Word: | |
Class: | |
Precautionary Statements: | |
UN#: | |
Hazard Statements: | |
Packing Group: | |
Application In Synthesis of [ 60612-00-2 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 60612-00-2 ]
- 1
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[ 13482-22-9 ]
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[ 122-51-0 ]
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[ 60612-00-2 ]
Yield | Reaction Conditions | Operation in experiment |
89% |
With toluene-4-sulfonic acid; In ethanol; at 20℃; |
Reference Example 14 [0451] Step 1 [0452] To a solution of <strong>[13482-22-9]4-hydroxycyclohexanone</strong> (2.0g, 17.5mmol) in ethanol (8ml) were added triethyl orthoformate (8.78ml, 52.6mmol) and p-toluenesulfonic acid monohydrate (3.3mg, 0.018mmol), and the mixture was stirred overnight at room temperature. To the reaction mixture was added saturated aqueous sodium bicarbonate, and the resulting mixture was extracted with ethyl acetate. The organic layer was dried over anhydrous sodium sulphate, and concentrated in vacuo. The resulting residue was purified by silica gel column chromatography (hexane-ethyl acetate) to give Compound vii-7 (2.93g, Yield 89%). [0453] 1H-NMR(CDCl3)delta:1.15-1.21 (m, 6H), 1.49-1.60 (m, 4H), 1.76-1.81 (m, 2H), 1.93-2.00 (m, 2H), 3.43-3.50 (m, 4H), 3.77 (brs, 1H). |
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