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CAS No. : | 47593-50-0 | MDL No. : | MFCD00625984 |
Formula : | C22H18O6 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | AYEXKJKXZHOWPW-UHFFFAOYSA-N |
M.W : | 378.37 | Pubchem ID : | 1204453 |
Synonyms : |
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Signal Word: | Warning | Class: | N/A |
Precautionary Statements: | P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313 | UN#: | N/A |
Hazard Statements: | H315-H319 | Packing Group: | N/A |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
74% | With NaOH In water High Pressure; mixt. of 1,4-bis(2-(pyridin-2-yl)-1H-imidazol-1-yl)butane, ligand, Cd(CH3CO2)2*2H2O, NaOH, H2O stirred for 1 h, sealed in autoclave, heated at 150°C for 72 h, cooled to 100°C at 10°C/h, held for 8 h, cooled to 30°C; collected; elem. anal.; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
60% | In water; N,N-dimethyl-formamide at 145℃; for 48h; High pressure; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
60% | In N,N-dimethyl-formamide at 145℃; for 48h; High pressure; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
40% | In water; N,N-dimethyl-formamide at 145℃; for 48h; High pressure; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
48% | In N,N-dimethyl-formamide at 145℃; for 48h; High pressure; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
45% | In water; N,N-dimethyl-formamide at 145℃; for 48h; High pressure; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
50% | In N,N-dimethyl-formamide at 145℃; for 48h; High pressure; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
52% | In N,N-dimethyl-formamide at 145℃; for 48h; High pressure; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
85% | With potassium hydroxide In methanol; water at 80℃; for 12h; Inert atmosphere; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
72% | With hydrogenchloride; N,N-dimethyl acetamide at 120℃; for 24h; Autoclave; | 2.2. Preparation of complexes Ln-MOF General procedure: LnCl 3*6H 2 O, (0.1 mmol), H 2 PMBB (0.045 g, 0.12 mmol), H 2 O (10 mL), DMA (10 mL) and HCl (1 M, 3 mL) were placed in a 25 mL Teflon-lined stainless-steel autoclave, and the resulted sus- pension was heated at 120 °C for 1 d. Furthermore, the autoclave was placed at room temperature. Colorless prism crystals appropri- ate for single crystal X-ray diffraction analysis were collected from the precipitation of reaction solution. The final reaction system was filtrated, and the solids were rinsed several times with H 2 O and methanol, and dried in air at ambient temperature. EuCl 3 ·6H 2 O (0.037 g), yield, 72% (based on Eu III ); IR (neat): 1601 (s), 1586 (s), 1532 (s), 1422 (s), 1387 (s), 1372 (s), 1293 (s), 1241 (s), 1174 (s), 1146 (s), 1100 (s), 1006 (s), 874 (s), 846 (s), 800 (s), 782 (s), 695 (s), 639 (s), 630 (s), 550 (s), 531 (s) cm -1 ; element analysis (%): calcd. for C 33 H 28 O 11 Eu: C 52.67, H 3.75; found: C 53.01, H 3.80. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
76% | With hydrogenchloride; N,N-dimethyl acetamide at 120℃; for 24h; Autoclave; | 2.2. Preparation of complexes Ln-MOF General procedure: LnCl 3*6H 2 O, (0.1 mmol), H 2 PMBB (0.045 g, 0.12 mmol), H 2 O (10 mL), DMA (10 mL) and HCl (1 M, 3 mL) were placed in a 25 mL Teflon-lined stainless-steel autoclave, and the resulted sus- pension was heated at 120 °C for 1 d. Furthermore, the autoclave was placed at room temperature. Colorless prism crystals appropri- ate for single crystal X-ray diffraction analysis were collected from the precipitation of reaction solution. The final reaction system was filtrated, and the solids were rinsed several times with H 2 O and methanol, and dried in air at ambient temperature. |