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CAS No. : | 438247-28-0 | MDL No. : | |
Formula : | C18H39NiOP2Si | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 420.23 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
99% | In diethyl ether (N2); addn. of diphosphine to a soln. of nickel complex in Et2O at -50°C, stirring for 1 h at room temp.; evapn., extn. with petroleum ether, concn., cooling to -30°C; elem. anal.; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
99% | In diethyl ether (N2); addn. of diphosphine to a soln. of nickel complex in Et2O at -50°C, stirring for 1 h at room temp.; evapn., extn. with petroleum ether, concn., cooling to -30°C; elem. anal.; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 4 steps 1: tetrahydrofuran; diethyl ether 2: diethyl ether 3: tetrahydrofuran 4: diethyl ether; pyridine | ||
Multi-step reaction with 4 steps 1: tetrahydrofuran; diethyl ether 2: diethyl ether 3: not given 4: diethyl ether; pyridine |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: diethyl ether 2: diethyl ether |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: diethyl ether 2: diethyl ether |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 3 steps 1: diethyl ether 2: tetrahydrofuran 3: diethyl ether; pyridine | ||
Multi-step reaction with 3 steps 1: diethyl ether 2: not given 3: diethyl ether; pyridine |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: tetrahydrofuran 2: diethyl ether; pyridine |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: not given 2: diethyl ether; pyridine |