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3-(diphenylphosphino)propionic acid-gold(I)chloride[ No CAS ]
C27H24AuClNO2PS2[ No CAS ]
Yield
Reaction Conditions
Operation in experiment
58%
Stage #1: 3-(diphenylphosphino)propionic acid-gold(I)chloride With (chloromethylene)dimethyliminium chloride In dichloromethane at 0℃; for 2h;
Stage #2: 5-[(4-ethylphenyl)methylene]-2-thioxo-4-thiazolidinone With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃;
Stage #1: C14H11AuCl2N2O3 With (chloromethylene)dimethyliminium chloride In dichloromethane at 0℃; for 0.5h;
Stage #2: 5-[(4-ethylphenyl)methylene]-2-thioxo-4-thiazolidinone With N-ethyl-N,N-diisopropylamine In dichloromethane at 20℃; for 24h;