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[ CAS No. 372159-77-8 ] {[proInfo.proName]}

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Chemical Structure| 372159-77-8
Chemical Structure| 372159-77-8
Structure of 372159-77-8 * Storage: {[proInfo.prStorage]}
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Product Details of [ 372159-77-8 ]

CAS No. :372159-77-8 MDL No. :MFCD03425261
Formula : C15H19NO3 Boiling Point : -
Linear Structure Formula :- InChI Key :CNEFTNPXPQDBGA-UHFFFAOYSA-N
M.W : 261.32 Pubchem ID :44784970
Synonyms :

Safety of [ 372159-77-8 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 372159-77-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 372159-77-8 ]

[ 372159-77-8 ] Synthesis Path-Downstream   1~5

  • 1
  • [ 372159-77-8 ]
  • [ 1271802-68-6 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 5 steps 1: N-chloro-succinimide / <i>L</i>-proline / chloroform / 12 h / 4 °C 2: toluene / 110 °C 3: N,N-dimethyl-formamide / 12 h / 20 °C 4: 2-Trimethylsilylimidazole / acetonitrile / 3 h / 0 °C 5: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / 85 °C
  • 2
  • [ 372159-77-8 ]
  • [ 1271808-92-4 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: N-chloro-succinimide / <i>L</i>-proline / chloroform / 12 h / 4 °C 2: toluene / 110 °C
  • 3
  • [ 372159-77-8 ]
  • [ 1271808-89-9 ]
YieldReaction ConditionsOperation in experiment
With N-chloro-succinimide In chloroform at 4℃; for 12h; 16 To a solution of aldehyde 16.1 (2.55 g) in CHC13 (50 mL) was addedNCS (1.6 g) and L-proline (58 mg). The solution was stirred at 4 °C for 12 h. The mixture was concentrated in vacuo, and the resultant residue was purified by column chromatography (gradient 50% EtOAc in hexane) to afford compound 16.2.
  • 4
  • [ 372159-77-8 ]
  • [ 1271808-95-7 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 3 steps 1: N-chloro-succinimide / <i>L</i>-proline / chloroform / 12 h / 4 °C 2: toluene / 110 °C 3: N,N-dimethyl-formamide / 12 h / 20 °C
  • 5
  • [ 372159-77-8 ]
  • [ 1271808-98-0 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 4 steps 1: N-chloro-succinimide / <i>L</i>-proline / chloroform / 12 h / 4 °C 2: toluene / 110 °C 3: N,N-dimethyl-formamide / 12 h / 20 °C 4: 2-Trimethylsilylimidazole / acetonitrile / 3 h / 0 °C
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