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CAS No. : | 372159-77-8 | MDL No. : | MFCD03425261 |
Formula : | C15H19NO3 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | CNEFTNPXPQDBGA-UHFFFAOYSA-N |
M.W : | 261.32 | Pubchem ID : | 44784970 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P280-P301+P312-P302+P352-P305+P351+P338 | UN#: | |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 5 steps 1: N-chloro-succinimide / <i>L</i>-proline / chloroform / 12 h / 4 °C 2: toluene / 110 °C 3: N,N-dimethyl-formamide / 12 h / 20 °C 4: 2-Trimethylsilylimidazole / acetonitrile / 3 h / 0 °C 5: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 12 h / 85 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: N-chloro-succinimide / <i>L</i>-proline / chloroform / 12 h / 4 °C 2: toluene / 110 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With N-chloro-succinimide In chloroform at 4℃; for 12h; | 16 To a solution of aldehyde 16.1 (2.55 g) in CHC13 (50 mL) was addedNCS (1.6 g) and L-proline (58 mg). The solution was stirred at 4 °C for 12 h. The mixture was concentrated in vacuo, and the resultant residue was purified by column chromatography (gradient 50% EtOAc in hexane) to afford compound 16.2. |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 3 steps 1: N-chloro-succinimide / <i>L</i>-proline / chloroform / 12 h / 4 °C 2: toluene / 110 °C 3: N,N-dimethyl-formamide / 12 h / 20 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 4 steps 1: N-chloro-succinimide / <i>L</i>-proline / chloroform / 12 h / 4 °C 2: toluene / 110 °C 3: N,N-dimethyl-formamide / 12 h / 20 °C 4: 2-Trimethylsilylimidazole / acetonitrile / 3 h / 0 °C |
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