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CAS No. : | 365-00-4 | MDL No. : | |
Formula : | C15H10F2O2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 260.24 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Class: | ||
Precautionary Statements: | UN#: | ||
Hazard Statements: | Packing Group: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
65% | With xenon difluoride In dichloromethane Ambient temperature; | |
Multi-step reaction with 2 steps 1: 70.7 percent / xenon difluoride / hydrogen difluoride / CH2Cl2 / Ambient temperature 2: 68 percent / xenon difluoride / hydrogen difluoride / CH2Cl2 / Ambient temperature |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
90% | With Selectfluor In water; acetonitrile at 20℃; for 48h; | |
88% | With 1-fluoro-2,4,6-trimethylpyridinium trifluoromethanesulfonate; zinc(II) chloride In 1,2-dichloro-ethane at 60℃; for 18h; | |
78% | With Selectfluor In acetonitrile for 192h; Ambient temperature; |
78% | With water; Selectfluor at 70℃; chemoselective reaction; | |
78% | With Selectfluor In water; acetonitrile at 20℃; for 16h; Schlenk technique; Sealed tube; chemoselective reaction; | |
73% | With [bis(acetoxy)iodo]benzene; triethylamine tris(hydrogen fluoride) In acetonitrile at 40℃; for 16h; Inert atmosphere; | |
72% | With sodium carbonate; Selectfluor In acetonitrile at 20℃; for 72h; | |
71% | With xenon difluoride In dichloromethane Ambient temperature; | |
71% | With 1-fluoro-3,3-dimethyl-1,3-dihydro-1λ3-benzo[d][1,2]iodaoxole; triethylamine tris(hydrogen fluoride) In dichloromethane at 60℃; for 24h; Inert atmosphere; | |
70% | With sodium carbonate; Selectfluor; sodium chloride at 70℃; | |
68% | With 2,3,5-trimethyl-pyridine; zinc(II) chloride; 1-fluoro-4-hydroxy-1,4-diazoniabicyclo[2,2,2]octane-1,4-bis(tetrafluoroborate) In acetonitrile at 50℃; for 48h; | |
67% | With Genapol LRO; Selectfluor In water at 60℃; for 3h; | |
Multi-step reaction with 2 steps 1: 37 percent / caesium fluoroxysulphate / acetonitrile / 2 h / 30 °C 2: 68 percent / xenon difluoride / hydrogen difluoride / CH2Cl2 / Ambient temperature | ||
Multi-step reaction with 2 steps 1: 66 percent / xenon difluoride / hydrogen difluoride / CH2Cl2 / Ambient temperature 2: 68 percent / xenon difluoride / hydrogen difluoride / CH2Cl2 / Ambient temperature | ||
With Selectfluor In water; acetonitrile at 20℃; | ||
Multi-step reaction with 3 steps 1: acetonitrile / 20 °C / Darkness 2: Selectfluor / acetonitrile / 20 °C 3: Selectfluor / acetonitrile / 25 °C | ||
Multi-step reaction with 3 steps 1: acetonitrile / 20 °C / Darkness 2: Selectfluor / [D3]acetonitrile; water / 3.5 h / 20 °C 3: Selectfluor / acetonitrile / 25 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
81% | With Selectfluor In acetonitrile at 82℃; for 0.166667h; microwave irradiation; | |
1: 52% 2: 15% | With N-Fluoro-o-benzenedisulfonimide In dichloromethane for 2h; Ambient temperature; | |
1: 50% 2: 6% | With triethylamine pentahydrogen fluoride salt; 4-tolyl iodide electrolysis: smooth Pt sheets as the anode and the cathode, divided cell, 20 mA/h (vs. Ag/Ag(+)), 3.0 F/mol; |
1: 37% 2: 9.5% | With cesium fluoroxysulphate In acetonitrile at 30℃; for 2h; | |
17 % Spectr. | With N-fluoro-4,6-bis(trifluoromethyl)pyridinium-2-sulfonate In various solvent(s) for 0.33h; Ambient temperature; Yields of byproduct given; | |
1: 10 % Spectr. 2: 76 % Spectr. | With trifluorormethanesulfonic acid; N,N’-difluoro-2,2’-bipyridinium bis(tetrafluoroborate) In acetonitrile for 48h; Heating; | |
With 1-fluoro-3,5-dichloropyridinium trifluoromethanesulfonate In 1,2-dichloro-ethane at 60℃; for 5h; | ||
66 % Spectr. | With N-fluoro-4,6-bis(trifluoromethyl)pyridinium-2-sulfonate In tetrahydrofuran for 16h; Ambient temperature; Yields of byproduct given; | |
With 1H-imidazole; zinc(II) chloride; 1-fluoro-4-hydroxy-1,4-diazoniabicyclo[2,2,2]octane-1,4-bis(tetrafluoroborate) In acetonitrile at 50℃; for 24h; | ||
1: 55 %Spectr. 2: 30 %Spectr. | With 1-fluoro-3,3-dimethyl-1,3-dihydro-1λ3-benzo[d][1,2]iodaoxole; triethylamine tris(hydrogen fluoride) In dichloromethane at 40℃; for 24h; Inert atmosphere; | |
With polyHIPE F-TEDA-OTf In acetonitrile at 20℃; for 72h; Green chemistry; Overall yield = 70.9 %Chromat.; | ||
With sodium carbonate; Selectfluor In neat (no solvent) for 2h; Milling; Overall yield = 93 %; Overall yield = 242 mg; | ||
With Selectfluor; acetonitrile; sodium chloride at 60℃; Overall yield = 90 %; Overall yield = 1.79 g; | ||
Multi-step reaction with 2 steps 1: acetonitrile / 20 °C / Darkness 2: Selectfluor / [D3]acetonitrile; water / 3.5 h / 20 °C |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
81% | With Selectfluor; triethylamine In acetonitrile at -10℃; for 0.5h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
84% | With hydrogen |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
89% | With 4-tert-butyl-2,6-dimethylphenylsulfur trifluoride; pyridine hydrofluoride In dichloromethane at 20℃; for 24h; Inert atmosphere; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
1: 64% 2: 15% 3: 9% | With triethylamine tris(hydrogen fluoride) In dichloromethane at 40℃; for 24h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
80% | With caesium carbonate In dimethyl sulfoxide at 20℃; for 12h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
83% | With caesium carbonate In dimethyl sulfoxide at 20℃; for 12h; | |
56% | With caesium carbonate In dimethyl sulfoxide for 1h; Milling; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
88% | With caesium carbonate In dimethyl sulfoxide at 20℃; for 12h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
47% | With caesium carbonate In dimethyl sulfoxide at 20℃; for 12h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
72% | With caesium carbonate In dimethyl sulfoxide at 80℃; for 12h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
92% | With caesium carbonate In dimethyl sulfoxide at 20℃; for 12h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
78% | With caesium carbonate In dimethyl sulfoxide at 20℃; for 12h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
81% | With caesium carbonate In dimethyl sulfoxide at 80℃; for 12h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
74% | With caesium carbonate In dimethyl sulfoxide at 20℃; for 12h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
89% | With caesium carbonate In dimethyl sulfoxide at 20℃; for 12h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
70% | With caesium carbonate In dimethyl sulfoxide at 80℃; for 12h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
51% | With caesium carbonate In toluene at 110℃; for 12h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
44% | With caesium carbonate In toluene at 110℃; for 12h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
92% | With caesium carbonate In dimethyl sulfoxide at 80℃; for 12h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
67% | With caesium carbonate In toluene at 110℃; for 12h; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
94% | Stage #1: di(p-nitrophenyl) disulfide; 2,2-difluoro-1,3-diphenyl-1,3-propanedione With caesium carbonate In toluene at 110℃; for 12h; Stage #2: With potassium hydroxide In water; toluene at 100℃; for 7h; |