Alternatived Products of [ 239113-48-5 ]
Product Details of [ 239113-48-5 ]
CAS No. : | 239113-48-5 |
MDL No. : | N/A |
Formula : |
-
|
Boiling Point : |
- |
Linear Structure Formula : | - |
InChI Key : | LHKOTTBRSICARI-UHFFFAOYSA-N |
M.W : |
-
|
Pubchem ID : | 10862783 |
Synonyms : |
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Safety of [ 239113-48-5 ]
Application In Synthesis of [ 239113-48-5 ]
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
- Downstream synthetic route of [ 239113-48-5 ]
- 1
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[ 921-26-6 ]
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[ 65355-14-8 ]
-
[ 239113-48-5 ]
Yield | Reaction Conditions | Operation in experiment |
50% |
With triethylamine In tetrahydrofuran at 20℃; for 20h; |
|
- 2
-
[ 65355-14-8 ]
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[ 108-18-9 ]
-
[ 239113-48-5 ]
Yield | Reaction Conditions | Operation in experiment |
67% |
Stage #1: diisopropylamine With triethylamine; phosphorus trichloride In dichloromethane at 0 - 20℃; for 3h; Inert atmosphere;
Stage #2: (S)-5,5',6,6',7,7',8,8'-octahydro-1,1'-bi-2-naphthol In dichloromethane for 12h; Inert atmosphere; |
|
|
Stage #1: diisopropylamine With triethylamine; phosphorus trichloride In dichloromethane at 0 - 20℃; Inert atmosphere;
Stage #2: (S)-5,5',6,6',7,7',8,8'-octahydro-1,1'-bi-2-naphthol In dichloromethane at 20℃; Inert atmosphere; |
|
Reference:
[1]Lee, Pin-Sheng; Yoshikai, Naohiko
[Organic Letters, 2015, vol. 17, # 1, p. 22 - 25]
[2]Zhu, Deng; Yu, Lu; Luo, Hui-Yun; Xue, Xiao-Song; Chen, Zhi-Min
[Angewandte Chemie - International Edition, 2022, vol. 61, # 42][Angew. Chem., 2022, vol. 134, # 42]
- 3
-
[ 239113-48-5 ]
-
[ 2851058-41-6 ]
Yield | Reaction Conditions | Operation in experiment |
140 mg |
With sulphur In dichloromethane at 20℃; Inert atmosphere; |
|
Reference:
[1]Zhu, Deng; Yu, Lu; Luo, Hui-Yun; Xue, Xiao-Song; Chen, Zhi-Min
[Angewandte Chemie - International Edition, 2022, vol. 61, # 42][Angew. Chem., 2022, vol. 134, # 42]