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CAS No. : | 238428-27-8 | MDL No. : | MFCD04039171 |
Formula : | C9H13ClN2O | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 200.67 | Pubchem ID : | - |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P261-P264-P270-P271-P280-P301+P312+P330-P302+P352-P304+P340+P312-P305+P351+P338-P332+P313-P337+P313-P362-P403+P233-P405-P501 | UN#: | |
Hazard Statements: | H302-H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
100% | With hydrogenchloride In 1,4-dioxane at 20℃; for 1h; | B; 2009.B To the intermediate from Step A above (333 mg) was added hydrogen chloride (4M in dioxane, 5 mL) and the suspension was stirred at room temperature for 1 h. The reaction mixture was evaporated to afford the title compound as colourless solid (251 mg; quantitative). [M-Cl]+=165. |
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