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[ CAS No. 2373-89-9 ] {[proInfo.proName]}

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Chemical Structure| 2373-89-9
Chemical Structure| 2373-89-9
Structure of 2373-89-9 * Storage: {[proInfo.prStorage]}
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Product Details of [ 2373-89-9 ]

CAS No. :2373-89-9 MDL No. :MFCD00025815
Formula : C17H16O3 Boiling Point : -
Linear Structure Formula :- InChI Key :HDXVSZWKIHQDES-LFYBBSHMSA-N
M.W : 268.31 Pubchem ID :5377817
Synonyms :

Safety of [ 2373-89-9 ]

Signal Word:Danger Class:9
Precautionary Statements:P201-P264-P280-P301+P330+P331-P312 UN#:3077
Hazard Statements:H302-H361-H372-H410 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 2373-89-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 2373-89-9 ]

[ 2373-89-9 ] Synthesis Path-Downstream   1~7

  • 1
  • [ 2373-89-9 ]
  • [ 14447-18-8 ]
  • [ 102238-09-5 ]
  • 2
  • [ 2373-89-9 ]
  • [ 3215-64-3 ]
  • [ 112425-47-5 ]
  • 3
  • [ 2373-89-9 ]
  • [ 3215-64-3 ]
  • 2-(2,4-Dichloro-phenyl)-3,5-bis-(4-methoxy-phenyl)-5-oxo-pentanenitrile [ No CAS ]
  • 4
  • [ 2373-89-9 ]
  • [ 76973-57-4 ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: 85 percent / hydrazine hydrate / ethanol / 5 h / Heating 2: 73 percent / Br2 / CHCl3 / 4 h / Ambient temperature
  • 5
  • [ 2373-89-9 ]
  • [ 75059-30-2 ]
YieldReaction ConditionsOperation in experiment
99% With sulfur; hydrazine hydrate In ethanol at 150℃; for 2h; Microwave irradiation;
  • 6
  • [ 2373-89-9 ]
  • [ 27126-76-7 ]
  • 2,3-di(4-methoxyphenyl)-1,1-ditosyloxypropan-3-one [ No CAS ]
YieldReaction ConditionsOperation in experiment
80% In dichloromethane at 40 - 42℃; stereoselective reaction; General procedure for the synthesis of ditosyloxy ketone derivatives (GP) General procedure: To the solution of chalcone 1 (0.004 mol) in dichloromethane (30-40 ml) was added HTIB (0.008 mol, 2 equiv.). Then theresulting mixture was allowed to stir at 40-42°C. HTIB was highly insoluble in dichloromethane, butgradually disappeared as the reaction proceeded. The stirring was allowed to continue for about 40-44hours. The solvent was evaporated in vacuo. The gummy mass so obtained was triturated withpetroleum ether (60-80°C) (3 x 20 ml) to remove iodobenzene. The white solid obtained was thoroughlywashed with water (2 x 30 ml) to remove p-toluenesulphonic acid formed as by-product. The solid wasrecrystalized from acetonitrile to give the pure ditosyloloxy ketone.
  • 7
  • [ 2373-89-9 ]
  • [ 1004-76-8 ]
  • 2,4-bis(4-methoxyphenyl)-8-thioxo-1,7,9-triazaspiro[4,5]dec-1-ene-6,10-dione [ No CAS ]
YieldReaction ConditionsOperation in experiment
89% With oxalic acid at 120℃; for 16h; regioselective reaction; Synthesis of 8-Thioxo-1,7,9-trizaospiro[4,5]dec-1-ene-6,10-dione Analogues General procedure: A mixture of α.β-unsaturated ketone (1 mmol), 5,6-diamino-2-mercaptopyrimidin-4-ol (1 mmol), and oxalic acid (20 mol%) was taken in an Ace Pressure tube, and the reaction mixture was heated at 120 °C for 16 h. After completion of the reaction (monitored by TLC), DMF (1 mL) was added to the gummy reaction mass and was stirred for 10 min at 120 °C to solubilize the reaction mass. The solution was cooled to room temperature and then poured into ice-cold water. The precipitate formed was filtered, dried, and purified by column chromatography using eluent ethyl acetate and hexane. All compounds were obtained as solids.
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