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[ CAS No. 2197-63-9 ] {[proInfo.proName]}

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Chemical Structure| 2197-63-9
Chemical Structure| 2197-63-9
Structure of 2197-63-9 * Storage: {[proInfo.prStorage]}
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Product Details of [ 2197-63-9 ]

CAS No. :2197-63-9 MDL No. :MFCD00008999
Formula : C32H67O4P Boiling Point : -
Linear Structure Formula :- InChI Key :RNPXCFINMKSQPQ-UHFFFAOYSA-N
M.W : 546.85 Pubchem ID :75143
Synonyms :
Dihexadecyl Phosphate;NSC 12429;Dicetyl Phosphate

Safety of [ 2197-63-9 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 2197-63-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Upstream synthesis route of [ 2197-63-9 ]

[ 2197-63-9 ] Synthesis Path-Upstream   1~5

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YieldReaction ConditionsOperation in experiment
11% at 80℃; Production Example 5; Synthesis of Dicetylphosphate; To a mixture of cetyl alcohol (19.50 g, 80.4 mmol) and benzene (100 ml), phosphorus oxychloride (2.5 ml, 26.8 mmol) was added dropwise at 80° C. (solvent reflux temperature) and further stirred for 12 hours. The solvent of the reaction solution was evaporated under a reduced pressure. To the obtained residue, benzene (50 ml) was added and cooled overnight. The precipitate generated was filtrated to obtain the titled compound (white powder, 1.64 g, 3.0 mmol, yield: 11percent).1H-NMR (ppm) δ: 0.87-0.89 (t, 6H), 1.25-1.37 (br, s, 52H), 1.65-1.72 (m, 4H), 4.00-4.06 (m4H), 7.05 (br, s, 1H)13C-NMR (ppm) δ: 14.11, 22.69, 25.44, 29.18, 29.36, 29.54, 29.61, 29.66, 29.67, 29.70, 29.71, 30.16, 30.21, 31.93, 67.69, 67.7331P-NMR (ppm) δ: 2.15SIMS mass analysis:Actual measurement value; 547.85Theoretical value; 547.83, relative to (C32H68O4P)+
Reference: [1] Patent: US2010/94020, 2010, A1, . Location in patent: Page/Page column 18
[2] Bulletin of the Chemical Society of Japan, 1978, vol. 51, p. 1877 - 1879
[3] Chemical and Pharmaceutical Bulletin, 1995, vol. 43, # 10, p. 1751 - 1754
[4] Bioconjugate Chemistry, 2010, vol. 21, # 5, p. 844 - 852
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Reference: [1] Patent: US2011/46408, 2011, A1, . Location in patent: Page/Page column 8
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Reference: [1] Journal of the Chemical Society, 1929, p. 298
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Reference: [1] Journal of the Chemical Society, 1955, p. 1584,1585
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  • [ 67-66-3 ]
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  • [ 1623-14-9 ]
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Reference: [1] Journal of the Chemical Society, 1929, p. 298
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