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[ CAS No. 1800552-46-8 ] {[proInfo.proName]}

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Chemical Structure| 1800552-46-8
Chemical Structure| 1800552-46-8
Structure of 1800552-46-8 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1800552-46-8 ]

CAS No. :1800552-46-8 MDL No. :MFCD32696917
Formula : C39H24N4 Boiling Point : -
Linear Structure Formula :- InChI Key :XVTLXVUSHIRJCS-UHFFFAOYSA-N
M.W : 548.63 Pubchem ID :122204474
Synonyms :

Safety of [ 1800552-46-8 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:N/A
Hazard Statements:H302-H315-H319-H335 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 1800552-46-8 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1800552-46-8 ]

[ 1800552-46-8 ] Synthesis Path-Downstream   1~6

  • 1
  • [ 4316-58-9 ]
  • [ 126747-14-6 ]
  • 4',4''',4'''''-nitrilotris(([1,1'-biphenyl]-4-carbonitrile)) [ No CAS ]
YieldReaction ConditionsOperation in experiment
80% With tetrabutylammomium bromide; potassium carbonate In water at 60℃; for 3h;
75% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In N,N-dimethyl-formamide at 90℃; for 48h; Inert atmosphere;
  • 2
  • [ CAS Unavailable ]
  • [ 1800552-46-8 ]
  • [ 2556942-42-6 ]
YieldReaction ConditionsOperation in experiment
78.6% Stage #1: dicyandiamide; 4',4''',4'''''-nitrilotris(([1,1'-biphenyl]-4-carbonitrile)) In 2-methoxy-ethanol at 20℃; for 0.5h; Inert atmosphere; Stage #2: With potassium hydroxide In 2-methoxy-ethanol at 125℃; for 24h; Inert atmosphere;
  • 3
  • [ CAS Unavailable ]
  • [ 171364-82-2 ]
  • [ 1800552-46-8 ]
YieldReaction ConditionsOperation in experiment
76% With tetrakis(triphenylphosphine) palladium(0); potassium carbonate In ethanol; toluene at 90℃; Inert atmosphere;
  • 4
  • [ 57774-35-3 ]
  • 4',4''',4'''''-nitrilotris(([1,1'-biphenyl]-4-carbonitrile)) [ No CAS ]
  • 5
  • [ 2762813-48-7 ]
  • [ 126747-14-6 ]
  • [ 1800552-46-8 ]
YieldReaction ConditionsOperation in experiment
55.1% With tetrakis-(triphenylphosphine)-palladium; potassium carbonate In ethanol; water monomer; toluene for 4h; Reflux; 29 Preparation 29: Synthesis of compound 2-173 (LT19-30-353) 9.7 g (19.2 mmol) of the intermediate (21) in a one-necked 500 mL flask,4-cyanophenylboronic acid (4-cyanophenylboronic acid) 8.5 g (57.7 mmol), Pd (PPh3) 41.3 g (1.2 mmol) and 80 mL toluene were added together and stirred, then 40 mL of ethanol, K2CO38.0 g (57.7 mmol) ) and 40 mL of distilled water were added, and the mixture was stirred under heating under reflux for 4 hours.When the reaction was completed, the reaction was cooled to room temperature, the solvent was blown off, and the solvent was removed by vacuum distillation after passing it through a celite pad with chloroform. Purification by column chromatography (HEX:CHCl3) gave 5.8 g (yield: 55.1%) of compound 2-173 (LT19-30-353) as a yellow solid.
  • 6
  • [ 4854-84-6 ]
  • 4',4''',4'''''-nitrilotris(([1,1'-biphenyl]-4-carbonitrile)) [ No CAS ]
YieldReaction ConditionsOperation in experiment
Multi-step reaction with 2 steps 1: Palladium(0) bis(dibenzylideneacetone); sodium tertiary butoxide; 1,1'-bis(diphenylphosphanyl)ferrocene / toluene / 8 h 2: tetrakis-(triphenylphosphine)-palladium; potassium carbonate / ethanol; toluene; water monomer / 4 h / Reflux
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