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CAS No. : | 1762-36-3 | MDL No. : | MFCD06661494 |
Formula : | C16H16N2O4 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | ARVRLHODKKEDGY-UHFFFAOYSA-N |
M.W : | 300.31 | Pubchem ID : | 400492 |
Synonyms : |
|
Signal Word: | Warning | Class: | |
Precautionary Statements: | P302+P352-P305+P351+P338 | UN#: | |
Hazard Statements: | H315-H319-H335 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
2,2'-Dipyridyl-5,5'-dicarbonsaeure I, Ethanol, H2SO4; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
In toluene for 3h; Heating; | ||
With thionyl chloride for 3h; Heating; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
1: 81% 2: 4% 3: 12% | Stage #1: 3,3'-bis(hydroxycarbonyl)-2,2'-bipyridine With thionyl chloride; chlorine for 1h; Heating; Stage #2: ethanol In toluene for 3h; Heating; | |
1: 45% 2: 12% 3: 39% | With thionyl chloride; chlorine for 5h; Heating; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: SOCl2 / 5 h / Heating 2: SOCl2 / 3 h / Heating |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
70.3% | In water reflux a suspn. of ligand and platinum complex in water for 18 h, cooling (as in: Dholakia, S., Gillard, R. D., Wimmer, F. L. Polyhedron 1985, 4, 791); elem. anal.; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
With sulfuric acid at 115℃; | ||
With hydrogenchloride Heating; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
670 mg | In toluene for 3h; Reflux; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
1.64 g | at 20℃; for 72h; Inert atmosphere; |
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 2 steps 1: water 2: methanol; acetonitrile |