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[ CAS No. 1639134-02-3 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 1639134-02-3
Chemical Structure| 1639134-02-3
Structure of 1639134-02-3 * Storage: {[proInfo.prStorage]}
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Product Details of [ 1639134-02-3 ]

CAS No. :1639134-02-3 MDL No. :N/A
Formula : C34H20O4S4 Boiling Point : -
Linear Structure Formula :- InChI Key :RLELZGCAYDJDTI-UHFFFAOYSA-N
M.W : 620.78 Pubchem ID :129896763
Synonyms :

Safety of [ 1639134-02-3 ]

Signal Word:Warning Class:
Precautionary Statements:P261-P280-P301+P312-P302+P352-P305+P351+P338 UN#:
Hazard Statements:H302-H315-H319-H335 Packing Group:
GHS Pictogram:

Application In Synthesis of [ 1639134-02-3 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 1639134-02-3 ]

[ 1639134-02-3 ] Synthesis Path-Downstream   1~6

  • 1
  • [ 33228-45-4 ]
  • 2,3,6,7-tetra(4-formylphenyl)tetrathiafulvalene [ No CAS ]
  • C82H88N4S4 [ No CAS ]
  • 2
  • [ 31366-25-3 ]
  • [ 1122-91-4 ]
  • 2,3,6,7-tetra(4-formylphenyl)tetrathiafulvalene [ No CAS ]
YieldReaction ConditionsOperation in experiment
40% With palladium diacetate; PtBu<SUB>3</SUB>HBF<SUB>4</SUB>; caesium carbonate In tetrahydrofuran for 48h; Reflux; Inert atmosphere;
38% With palladium diacetate; caesium carbonate; tri tert-butylphosphoniumtetrafluoroborate In tetrahydrofuran for 48h; Inert atmosphere; Reflux;
36% With tris(isopropyl)phosphonium tetrafluoroborate; palladium diacetate; caesium carbonate In tetrahydrofuran for 24h; Inert atmosphere; Reflux;
30% With palladium diacetate; caesium carbonate; tri tert-butylphosphoniumtetrafluoroborate In tetrahydrofuran at 75℃; for 30h; Schlenk technique; Inert atmosphere;
25% With tri-tert-butylphosphonium tetrafluoroborate; palladium diacetate; caesium carbonate In tetrahydrofuran for 15h; Reflux; Inert atmosphere;

  • 3
  • [ 1639134-02-3 ]
  • [ 62-53-3 ]
  • [ 1807606-81-0 ]
YieldReaction ConditionsOperation in experiment
94% In toluene at 130℃; for 5h; Dean-Stark;
  • 4
  • [ CAS Unavailable ]
  • [ 1639134-02-3 ]
  • [ CAS Unavailable ]
YieldReaction ConditionsOperation in experiment
70% With acetic acid In water; 1,2-dichloro-benzene at 140℃; for 120h; Sonication; Sealed tube; 1 Example 1 5 mg (0.01 mmol) of tetrakis tetrahedral configuration of tetrakis(4-anilino)adamantane (TAPA) and 6.2 mg (0.01 mmol)Tetrakis(p-butyryl)tetrathiafulvalene (TTF-Ph-CHO) was added to an ampoule, 1 mL of o-dichlorobenzene was added, ultrasonically mixed uniformly, and then 0.1 mL (6 mol/L) of aqueous acetic acid solution was added. The ampoule was placed in liquid nitrogen for freezing, vacuumed and flame sealed, sealed in an oven, and heated to 140 ° C for 5 days. After the reaction is completed, the obtained solid is transferred to a centrifuge tube.The mixture was washed 5 times with N,N-dimethylformamide and tetrahydrofuran, and dried under vacuum at 80 ° C for 12 h to obtain 7 mg of dark red solid powder COF-TTF-Ad in a yield of 70%.
  • 5
  • 2,3,6,7-tetra(4-formylphenyl)tetrathiafulvalene [ No CAS ]
  • [ 16004-77-6 ]
  • C74H92N16S4 [ No CAS ]
YieldReaction ConditionsOperation in experiment
75% With acetic acid In water; 1,2-dichloro-benzene; butan-1-ol at 120℃; for 72h; Sealed tube;
  • 6
  • [ 60532-63-0 ]
  • [ 1639134-02-3 ]
  • [ CAS Unavailable ]
YieldReaction ConditionsOperation in experiment
78% With acetic acid In water; 1,2-dichloro-benzene; butan-1-ol at 120℃; for 72h; Sealed tube;
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