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CAS No. : | 1613192-01-0 | MDL No. : | MFCD29053447 |
Formula : | C15H22FN3O2 | Boiling Point : | - |
Linear Structure Formula : | - | InChI Key : | - |
M.W : | 295.35 | Pubchem ID : | - |
Synonyms : |
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Signal Word: | Warning | Class: | |
Precautionary Statements: | P501-P270-P264-P280-P302+P352-P337+P313-P305+P351+P338-P362+P364-P332+P313-P301+P312+P330 | UN#: | |
Hazard Statements: | H302-H315-H319 | Packing Group: | |
GHS Pictogram: |
* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.
Yield | Reaction Conditions | Operation in experiment |
---|---|---|
Multi-step reaction with 3 steps 1: pyridine / 95 °C / Inert atmosphere 2: hydrogenchloride / water; 1,4-dioxane / Inert atmosphere 3: N-[(6-chlorobenzotriazol-1-yl)oxy-(dimethylamino)methylene]-dimethyl-ammonium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / Inert atmosphere | ||
Multi-step reaction with 4 steps 1: pyridine / 95 °C / Inert atmosphere 2: triethylsilane / dichloromethane / 20 - 40 °C 3: hydrogenchloride / 1-methyl-pyrrolidin-2-one; 1,4-dioxane / 0.33 h / 20 °C 4: N-[(6-chlorobenzotriazol-1-yl)oxy-(dimethylamino)methylene]-dimethyl-ammonium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / Inert atmosphere | ||
Multi-step reaction with 3 steps 1: pyridine / 16 h / 90 - 100 °C 2: acetonitrile / 16 h / 75 - 80 °C 3: N-[(6-chlorobenzotriazol-1-yl)oxy-(dimethylamino)methylene]-dimethyl-ammonium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / Inert atmosphere |
Multi-step reaction with 3 steps 1: pyridine / 95 °C / Inert atmosphere 2: acetonitrile / 16 h / 75 - 80 °C 3: N-[(6-chlorobenzotriazol-1-yl)oxy-(dimethylamino)methylene]-dimethyl-ammonium tetrafluoroborate; N-ethyl-N,N-diisopropylamine / tetrahydrofuran / Inert atmosphere |