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[ CAS No. 150405-69-9 ] {[proInfo.proName]}

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Cat. No.: {[proInfo.prAm]}
Chemical Structure| 150405-69-9
Chemical Structure| 150405-69-9
Structure of 150405-69-9 * Storage: {[proInfo.prStorage]}
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Product Details of [ 150405-69-9 ]

CAS No. :150405-69-9 MDL No. :MFCD00799419
Formula : C30H27N3 Boiling Point : -
Linear Structure Formula :- InChI Key :ZVFQEOPUXVPSLB-UHFFFAOYSA-N
M.W : 429.56 Pubchem ID :11441792
Synonyms :
UV :290 nm (in THF)
FL :370 nm (in THF) Materials Type :Other OLED Materials

Safety of [ 150405-69-9 ]

Signal Word:Warning Class:N/A
Precautionary Statements:P280-P305+P351+P338 UN#:N/A
Hazard Statements:H302 Packing Group:N/A
GHS Pictogram:

Application In Synthesis of [ 150405-69-9 ]

* All experimental methods are cited from the reference, please refer to the original source for details. We do not guarantee the accuracy of the content in the reference.

  • Downstream synthetic route of [ 150405-69-9 ]

[ 150405-69-9 ] Synthesis Path-Downstream   1~1

  • 1
  • [ 150405-69-9 ]
  • [ 22445-41-6 ]
  • C46H43N3 [ No CAS ]
  • C38H35N3 [ No CAS ]
  • C38H35N3 [ No CAS ]
YieldReaction ConditionsOperation in experiment
42% With C17H24N5Ru(1+)*F6P(1-); potassium acetate; potassium carbonate In 1-methyl-pyrrolidin-2-one at 50℃; for 72h; Inert atmosphere;
42% With C17H24N5Ru(1+)*F6P(1-); potassium acetate; potassium carbonate In 1-methyl-pyrrolidin-2-one at 50℃; for 72h; Inert atmosphere; Glovebox; General Procedure C: arylation of DG-containing (hetero)arenes with (hetero)aryl (pseudo)halides using cyclometalated ruthenium(ll) catalysts General procedure: Unless otherwise stated, in an Argon filled glove-box a crimp-cap microwave vial equipped with a magnetic stirring bar was charged with the appropriate cyclometalated Ru(ll)-catalyst (like Ru1-Ru46, from 3 mol % to 10 mol %), KOAc (5.9 mg, 0.06 mmol, 30 mol %), K2CO3 (2.0 - 4.0 equiv.), the appropriate DG-containing arene (like N1-N12, 0.20 mmol, 1.0 equiv.), the appropriate (hetero)aryl (pseudo)halide (like X1-X42, 0.2 mmol, 1.0 equiv) and /V-methyl-2- pyrrolidone (NMP) (200 pL, 1 M). The vial was capped and stirred at 35 °C for 24 hours. Upon completion, the crude mixture was loaded on a silica gel column and purified by flash chromatography
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